C₂₈H₂₄N₂O₄S

Base Information

Chemical Name:C₂₈H₂₄N₂O₄S
CAS No.:1423685-40-8
Molecular Formula:C₂₈H₂₄N₂O₄S
Molecular Weight:484.576
Hs Code.:

C<sub>28</sub>H<sub>24</sub>N<sub>2</sub>O<sub>4</sub>S

Synonyms:C₂₈H₂₄N₂O₄S

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Chemical Property of C₂₈H₂₄N₂O₄S

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Technology Process of C₂₈H₂₄N₂O₄S

There total 11 articles about C₂₈H₂₄N₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1423691-98-8
C₂₉H₂₆N₂O₄S

: 1423685-40-8
C₂₈H₂₄N₂O₄S

Guidance literature:: C₂₉H₂₆N₂O₄S; With sodium t-butanolate; In tetrahydrofuran; acetonitrile; at 20 ℃;

With hydrogenchloride; In tetrahydrofuran; acetonitrile; at 0 ℃; pH=4;

Reference yield:

: 124276-67-1
1-(4-bromophenyl)cyclopropanecarbonitrile

: 1423685-40-8
C₂₈H₂₄N₂O₄S

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide / ethylene glycol / 6 h / 160 °C

1.2: pH 3 - 4

2.1: sulfuric acid / 4 h / 65 °C

3.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 90 °C / Inert atmosphere

4.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 80 °C / Inert atmosphere

5.1: sodium t-butanolate / tetrahydrofuran; acetonitrile / 20 °C

5.2: 0 °C / pH 4

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sulfuric acid; sodium carbonate; potassium hydroxide; sodium t-butanolate; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; water; ethylene glycol; acetonitrile;

Reference yield:

: 345965-52-8
1-(4-bromophenyl)cyclopropanecarboxylic acid

: 1423685-40-8
C₂₈H₂₄N₂O₄S

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid / 4 h / 65 °C

2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 90 °C / Inert atmosphere

3.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 80 °C / Inert atmosphere

4.1: sodium t-butanolate / tetrahydrofuran; acetonitrile / 20 °C

4.2: 0 °C / pH 4

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sulfuric acid; sodium carbonate; sodium t-butanolate; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; water; acetonitrile;