(7E,15E)-5,13-ditosyl-5,6,13,14-tetrahydrodibenzo[b,h][1,7]diazacyclododecine

Base Information

• Chemical Name: (7E,15E)-5,13-ditosyl-5,6,13,14-tetrahydrodibenzo[b,h][1,7]diazacyclododecine
• CAS No.: 1038502-69-0
• Molecular Formula: C₃₂H₃₀N₂O₄S₂
• Molecular Weight: 570.733

Synonyms:(7E,15E)-5,13-ditosyl-5,6,13,14-tetrahydrodibenzo[b,h][1,7]diazacyclododecine

Chemical Property of (7E,15E)-5,13-ditosyl-5,6,13,14-tetrahydrodibenzo[b,h][1,7]diazacyclododecine

Chemical Property:

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Technology Process of (7E,15E)-5,13-ditosyl-5,6,13,14-tetrahydrodibenzo[b,h][1,7]diazacyclododecine

There total 1 articles about (7E,15E)-5,13-ditosyl-5,6,13,14-tetrahydrodibenzo[b,h][1,7]diazacyclododecine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

1-tosyl-4-vinyl-1,4-dihydro-2H-benzo[d] [1,3]oxazin-2-one (1038502-72-5) → (7E,15E)-5,13-ditosyl-5,6,13,14-tetrahydrodibenzo[b,h][1,7]diazacyclododecine (1038502-69-0)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 20 ℃; for 0.166667h; Inert atmosphere;

DOI:10.1021/ja801742h

Reference yield: 100.0%

(7E,15E)-5,13-ditosyl-5,6,13,14-tetrahydrodibenzo[b,h][1,7]diazacyclododecine (1038502-69-0) → 1-tosyl-1, 2-dihydroquinoline (13268-54-7)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; -butyl vinyl ether; In toluene; Inert atmosphere; Heating;

DOI:10.1016/j.tet.2009.04.071

upstream raw materials:

1-tosyl-4-vinyl-1,4-dihydro-2H-benzo[d] [1,3]oxazin-2-one

Downstream raw materials:

1-tosyl-1, 2-dihydroquinoline

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