[3-(3-benzyloxycarbonylaminopropylamino)propyl]carbamic acid benzyl ester

Base Information

• Chemical Name: [3-(3-benzyloxycarbonylaminopropylamino)propyl]carbamic acid benzyl ester
• CAS No.: 183249-68-5
• Molecular Formula: C₂₂H₂₉N₃O₄
• Molecular Weight: 399.49

Synonyms:[3-(3-benzyloxycarbonylaminopropylamino)propyl]carbamic acid benzyl ester

Chemical Property of [3-(3-benzyloxycarbonylaminopropylamino)propyl]carbamic acid benzyl ester

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

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Technology Process of [3-(3-benzyloxycarbonylaminopropylamino)propyl]carbamic acid benzyl ester

There total 5 articles about [3-(3-benzyloxycarbonylaminopropylamino)propyl]carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.1%

bis(3-aminopropyl)amine (56-18-8) + benzyl chloroformate (501-53-1,94274-21-2) → [3-(3-benzyloxycarbonylaminopropylamino)propyl]carbamic acid benzyl ester (183249-68-5)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 10 ℃; Temperature; Reagent/catalyst; Solvent;

Reference yield: 77.0%

bis(3-aminopropyl)amine (56-18-8) + benzyl phenyl carbonate (28170-07-2) → [3-(3-benzyloxycarbonylaminopropylamino)propyl]carbamic acid benzyl ester (183249-68-5)

Guidance literature:

In dichloromethane; at 20 ℃;

DOI:10.1055/s-2002-34859

Reference yield: 72.0%

bis(3-aminopropyl)amine (56-18-8) + benzyl cyanoformate (5532-86-5) → [3-(3-benzyloxycarbonylaminopropylamino)propyl]carbamic acid benzyl ester (183249-68-5)

Guidance literature:

In dichloromethane; at 25 ℃; for 2h;

DOI:10.1021/jo961047z DOI:10.1021/ja963874n

upstream raw materials:

bis(3-aminopropyl)amine

benzyl cyanoformate

benzyl phenyl carbonate

1,1'-carbonyldiimidazole

Downstream raw materials:

[Bis-(3-benzyloxycarbonylamino-propyl)-amino]-acetic acid tert-butyl ester

N,N-Bis-(3-benzyloxycarbonylamino-propyl)-succinamic acid

bis(3-benzyloxycarbonylaminopropyl)-N-tert-butoxycarbonylamine

C₂₈H₃₃N₅O₇

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