N,N'-diphenyl-1,1,3,3,5,5-hexamethyl-1,3,5-trisila-2,4-diaza-6-oxacyclohexane

Base Information

Chemical Name:N,N'-diphenyl-1,1,3,3,5,5-hexamethyl-1,3,5-trisila-2,4-diaza-6-oxacyclohexane
CAS No.:54006-36-9
Molecular Formula:C₁₈H₂₈N₂OSi₃
Molecular Weight:372.69
Hs Code.:

Synonyms:N,N'-diphenyl-1,1,3,3,5,5-hexamethyl-1,3,5-trisila-2,4-diaza-6-oxacyclohexane

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Chemical Property of N,N'-diphenyl-1,1,3,3,5,5-hexamethyl-1,3,5-trisila-2,4-diaza-6-oxacyclohexane

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Technology Process of N,N'-diphenyl-1,1,3,3,5,5-hexamethyl-1,3,5-trisila-2,4-diaza-6-oxacyclohexane

There total 1 articles about N,N'-diphenyl-1,1,3,3,5,5-hexamethyl-1,3,5-trisila-2,4-diaza-6-oxacyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54006-36-9
N,N'-diphenyl-1,1,3,3,5,5-hexamethyl-1,3,5-trisila-2,4-diaza-6-oxacyclohexane

Guidance literature:: Anilin 1. 1,3-Dichlor-tetramethyl-siloxan 2. Dichlor-dimethyl-silan, Et3N, DMF;

Reference yield: 39.0%

: 17933-16-3
dibromomethylborane

: 54006-36-9
N,N'-diphenyl-1,1,3,3,5,5-hexamethyl-1,3,5-trisila-2,4-diaza-6-oxacyclohexane

: 81720-62-9
3,5-diphenylcyclo-1-oxa-3,5-diaza-2,4,6-trimethyl-2,4,6-triborane

Guidance literature:: In dichloromethane; byproducts: (CH3)3SiBr; under N2, to soln. of O(SiMe2NPh)2SiMe2 (0.033 mole) in CH2Cl2 added dropwise at -80°C MeBBr2, warmed to room temp., refluxed for 3 h; evapn., sublimation;
DOI:10.1016/0022-328X(85)80026-7

Reference yield:

: 67-56-1
methanol

: 54006-36-9
N,N'-diphenyl-1,1,3,3,5,5-hexamethyl-1,3,5-trisila-2,4-diaza-6-oxacyclohexane

: 62-53-3
aniline

: 109756-02-7
1-methoxy-2-phenyl-1,1,3,3-tetramethyl-3-(methoxydimethyl)siloxydisilazane

Guidance literature:: With acetate buffer; In water; at 25 ℃; Rate constant; effect of various acetate buffer concentrations; ΔH(excit.); ΔS(excit.);
DOI:10.1016/0022-328X(86)80214-5