C₂₆H₃₄ClN₅O₂

Base Information

Chemical Name:C₂₆H₃₄ClN₅O₂
CAS No.:416849-76-8
Molecular Formula:C₂₆H₃₄ClN₅O₂
Molecular Weight:484.041
Hs Code.:

C<sub>26</sub>H<sub>34</sub>ClN<sub>5</sub>O<sub>2</sub>

Synonyms:C₂₆H₃₄ClN₅O₂

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Chemical Property of C₂₆H₃₄ClN₅O₂

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Technology Process of C₂₆H₃₄ClN₅O₂

There total 10 articles about C₂₆H₃₄ClN₅O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 416852-65-8
C₃₀H₃₉ClN₄O₄

: 593-56-6
N-methoxylamine hydrochloride

: 416849-76-8
C₂₆H₃₄ClN₅O₂

: 416849-77-9
C₂₉H₃₈ClN₅O₄

Guidance literature:: C₃₀H₃₉ClN₄O₄; N-methoxylamine hydrochloride; In pyridine; ethanol; for 18h; Heating / reflux;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 18h;

Reference yield:

: 304873-62-9
(4-hydroxymethylpyridin-2-yl)carbamic acid tert-butyl ester

: 416849-76-8
C₂₆H₃₄ClN₅O₂

: 416849-77-9
C₂₉H₃₈ClN₅O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; sodium bromide / dichloromethane; water / 1 h / 0 °C

2.1: acetic acid / dichloromethane / 0.67 h / 20 °C

2.2: 20 °C

3.1: lithium hydroxide; water / tetrahydrofuran; methanol / 20 °C

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 18 h / 20 °C

5.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / 0.67 h / -70 °C

6.1: pyridine; ethanol / 18 h / Heating / reflux

6.2: 18 h / 20 °C

With lithium hydroxide; sodium hypochlorite; oxalyl dichloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; water; sodium hydrogencarbonate; benzotriazol-1-ol; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium bromide; acetic acid; In tetrahydrofuran; pyridine; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 695-34-1
2-Amino-4-methylpyridine

: 416849-76-8
C₂₆H₃₄ClN₅O₂

: 416849-77-9
C₂₉H₃₈ClN₅O₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: tert-butyl alcohol / 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 2.5 h / -78 - 20 °C

2.2: 48 h / -78 - 20 °C

3.1: sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; sodium bromide / dichloromethane; water / 1 h / 0 °C

4.1: acetic acid / dichloromethane / 0.67 h / 20 °C

4.2: 20 °C

5.1: lithium hydroxide; water / tetrahydrofuran; methanol / 20 °C

6.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 18 h / 20 °C

7.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / 0.67 h / -70 °C

8.1: pyridine; ethanol / 18 h / Heating / reflux

8.2: 18 h / 20 °C

With lithium hydroxide; sodium hypochlorite; n-butyllithium; oxalyl dichloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; water; sodium hydrogencarbonate; benzotriazol-1-ol; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium bromide; acetic acid; In tetrahydrofuran; pyridine; methanol; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;