(S)-2-[4-(6,7-Bis-hexadecanoyloxy-heptanoylamino)-benzoylamino]-pentanedioic acid di-tert-butyl ester

Base Information

Chemical Name:(S)-2-[4-(6,7-Bis-hexadecanoyloxy-heptanoylamino)-benzoylamino]-pentanedioic acid di-tert-butyl ester
CAS No.:186807-28-3
Molecular Formula:C₅₉H₁₀₂N₂O₁₀
Molecular Weight:999.466
Hs Code.:

Synonyms:(S)-2-[4-(6,7-Bis-hexadecanoyloxy-heptanoylamino)-benzoylamino]-pentanedioic acid di-tert-butyl ester

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Chemical Property of (S)-2-[4-(6,7-Bis-hexadecanoyloxy-heptanoylamino)-benzoylamino]-pentanedioic acid di-tert-butyl ester

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Technology Process of (S)-2-[4-(6,7-Bis-hexadecanoyloxy-heptanoylamino)-benzoylamino]-pentanedioic acid di-tert-butyl ester

There total 4 articles about (S)-2-[4-(6,7-Bis-hexadecanoyloxy-heptanoylamino)-benzoylamino]-pentanedioic acid di-tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 186807-27-2
(S)-2-[4-(6,7-Dihydroxy-heptanoylamino)-benzoylamino]-pentanedioic acid di-tert-butyl ester

: 112-67-4
n-hexadecanoyl chloride

: 186807-28-3
(S)-2-[4-(6,7-Bis-hexadecanoyloxy-heptanoylamino)-benzoylamino]-pentanedioic acid di-tert-butyl ester

Guidance literature:: With dmap; In dichloromethane; for 1h; Ambient temperature;
DOI:10.1248/cpb.46.255

Reference yield:

: 1119-60-4
hept-6-enoic acid

: 186807-28-3
(S)-2-[4-(6,7-Bis-hexadecanoyloxy-heptanoylamino)-benzoylamino]-pentanedioic acid di-tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / pyridine, PCl₃ / 0.5 h / Ambient temperature

2: 90 percent / N-methylmorpholine-N-oxide, OsO₄ / acetone; tetrahydrofuran; H₂O / 10 h / Ambient temperature

3: 87 percent / DMAP / CH₂Cl₂ / 1 h / Ambient temperature

With pyridine; dmap; osmium(VIII) oxide; 4-methylmorpholine N-oxide; phosphorus trichloride; In tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1248/cpb.46.255

Reference yield:

: 76282-66-1
di-tert-butyl (S)-N-(p-aminobenzoyl)-glutamate

: 186807-28-3
(S)-2-[4-(6,7-Bis-hexadecanoyloxy-heptanoylamino)-benzoylamino]-pentanedioic acid di-tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / pyridine, PCl₃ / 0.5 h / Ambient temperature

2: 90 percent / N-methylmorpholine-N-oxide, OsO₄ / acetone; tetrahydrofuran; H₂O / 10 h / Ambient temperature

3: 87 percent / DMAP / CH₂Cl₂ / 1 h / Ambient temperature

With pyridine; dmap; osmium(VIII) oxide; 4-methylmorpholine N-oxide; phosphorus trichloride; In tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1248/cpb.46.255