7-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-2-(ethylthio)-5,6-diphenyl-3Hpyrrolo[2,3-d]pyrimidine-4(7H)-one

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Chemical Name:7-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-2-(ethylthio)-5,6-diphenyl-3Hpyrrolo[2,3-d]pyrimidine-4(7H)-one
CAS No.:1354047-25-8
Molecular Formula:C₃₁H₂₇N₅O₂S
Molecular Weight:533.654
Hs Code.:

Synonyms:7-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-2-(ethylthio)-5,6-diphenyl-3Hpyrrolo[2,3-d]pyrimidine-4(7H)-one

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Chemical Property of 7-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-2-(ethylthio)-5,6-diphenyl-3Hpyrrolo[2,3-d]pyrimidine-4(7H)-one

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Technology Process of 7-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-2-(ethylthio)-5,6-diphenyl-3Hpyrrolo[2,3-d]pyrimidine-4(7H)-one

There total 4 articles about 7-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-2-(ethylthio)-5,6-diphenyl-3Hpyrrolo[2,3-d]pyrimidine-4(7H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1354047-22-5
7-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-5,6-diphenyl-2-thioxo-2,3-dihydro-1H-pyrrolo[2,3-d]pyrimidine-4(7H)-one

: 75-03-6
ethyl iodide

: 1354047-25-8
7-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-2-(ethylthio)-5,6-diphenyl-3Hpyrrolo[2,3-d]pyrimidine-4(7H)-one

Guidance literature:: 7-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-5,6-diphenyl-2-thioxo-2,3-dihydro-1H-pyrrolo[2,3-d]pyrimidine-4(7H)-one; With sodium; In ethanol; at 20 ℃; for 0.333333h;

With sodium ethanolate; for 5.5h; Reflux;

ethyl iodide;
DOI:10.1111/j.1747-0285.2012.01440.x

Reference yield: 64.0%

: 1354047-22-5
7-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-5,6-diphenyl-2-thioxo-2,3-dihydro-1H-pyrrolo[2,3-d]pyrimidine-4(7H)-one

: 1354047-25-8
7-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-2-(ethylthio)-5,6-diphenyl-3Hpyrrolo[2,3-d]pyrimidine-4(7H)-one

Guidance literature:: With sodium ethanolate; for 5h; Reflux;
DOI:10.1002/ardp.201100056

Reference yield:

: 1354047-10-1
C₂₈H₂₃N₅O

: 1354047-25-8
7-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-2-(ethylthio)-5,6-diphenyl-3Hpyrrolo[2,3-d]pyrimidine-4(7H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; acetic acid; sodium nitrite / water / 8.5 h / 0 - 20 °C

2: ethanol / 10 h / Reflux

3: sodium ethanolate / 5 h / Reflux

With hydrogenchloride; sodium ethanolate; acetic acid; sodium nitrite; In ethanol; water;
DOI:10.1002/ardp.201100056