phenyl (1-(3-chlorophenyl)-3-(trifluoromethyl)-1H-pyrazol-5-yl)methylcarbamate

Base Information

Chemical Name:phenyl (1-(3-chlorophenyl)-3-(trifluoromethyl)-1H-pyrazol-5-yl)methylcarbamate
CAS No.:1360686-94-7
Molecular Formula:C₁₈H₁₃ClF₃N₃O₂
Molecular Weight:395.768
Hs Code.:

Synonyms:phenyl (1-(3-chlorophenyl)-3-(trifluoromethyl)-1H-pyrazol-5-yl)methylcarbamate

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Chemical Property of phenyl (1-(3-chlorophenyl)-3-(trifluoromethyl)-1H-pyrazol-5-yl)methylcarbamate

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Technology Process of phenyl (1-(3-chlorophenyl)-3-(trifluoromethyl)-1H-pyrazol-5-yl)methylcarbamate

There total 4 articles about phenyl (1-(3-chlorophenyl)-3-(trifluoromethyl)-1H-pyrazol-5-yl)methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1254713-79-5
(1-(3-chlorophenyl)-3-(trifluoromethyl)-1H-pyrazol-5-yl)methanamine

: 1885-14-9
phenyl chloroformate

: 1360686-94-7
phenyl (1-(3-chlorophenyl)-3-(trifluoromethyl)-1H-pyrazol-5-yl)methylcarbamate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 12h;

Reference yield:

: 108-42-9
3-chloro-aniline

: 1360686-94-7
phenyl (1-(3-chlorophenyl)-3-(trifluoromethyl)-1H-pyrazol-5-yl)methylcarbamate

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogenchloride; sodium nitrite; tin(II) chloride hydrate / water / 2 h / -5 - 0 °C

1.2: pH 9

2.1: ethanol / 5 h / Reflux

3.1: N-chloro-succinimide / N,N-dimethyl-formamide / 3 h / 20 °C

4.1: triethylamine / toluene / 20 h / 80 °C

5.1: hydrogen; ammonia / methanol / 80 °C / 7500.75 Torr

6.1: triethylamine / dichloromethane / 12 h / 20 °C

With hydrogenchloride; N-chloro-succinimide; tin(II) chloride hydrate; ammonia; hydrogen; triethylamine; sodium nitrite; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1254713-76-2
hydrazonoyl chloride

: 1360686-94-7
phenyl (1-(3-chlorophenyl)-3-(trifluoromethyl)-1H-pyrazol-5-yl)methylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / toluene / 20 h / 80 °C

2: hydrogen; ammonia / methanol / 80 °C / 7500.75 Torr

3: triethylamine / dichloromethane / 12 h / 20 °C

With ammonia; hydrogen; triethylamine; In methanol; dichloromethane; toluene;