(3,5-dioxohepta-1,6-diene-1,7-diyl)bis(2-methoxy-1,4-phenylene) diacetate

Base Information

Chemical Name:(3,5-dioxohepta-1,6-diene-1,7-diyl)bis(2-methoxy-1,4-phenylene) diacetate
CAS No.:98886-13-6
Molecular Formula:C₂₅H₂₄O₈
Molecular Weight:452.461
Hs Code.:

Synonyms:(3,5-dioxohepta-1,6-diene-1,7-diyl)bis(2-methoxy-1,4-phenylene) diacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3,5-dioxohepta-1,6-diene-1,7-diyl)bis(2-methoxy-1,4-phenylene) diacetate

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Technology Process of (3,5-dioxohepta-1,6-diene-1,7-diyl)bis(2-methoxy-1,4-phenylene) diacetate

There total 5 articles about (3,5-dioxohepta-1,6-diene-1,7-diyl)bis(2-methoxy-1,4-phenylene) diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 458-37-7
curcumin

: 108-24-7
acetic anhydride

: 98886-13-6
(3,5-dioxohepta-1,6-diene-1,7-diyl)bis(2-methoxy-1,4-phenylene) diacetate

Guidance literature:: With pyridine; dmap; at 0 - 20 ℃;
DOI:10.1080/14756366.2018.1488695

Reference yield: 70.1%

: 98885-93-9,115851-80-4,147556-16-9
curcumin

: 108-24-7
acetic anhydride

: 98886-13-6
(3,5-dioxohepta-1,6-diene-1,7-diyl)bis(2-methoxy-1,4-phenylene) diacetate

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 3h;
DOI:10.3390/molecules24050910

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 98886-13-6
(3,5-dioxohepta-1,6-diene-1,7-diyl)bis(2-methoxy-1,4-phenylene) diacetate

Guidance literature:: Multi-step reaction with 2 steps

1: triethyl borate; boron trioxide; piperidine / 1,4-dioxane

2: acetic anhydride; pyridine

With piperidine; pyridine; triethyl borate; acetic anhydride; boron trioxide; In 1,4-dioxane;
DOI:10.1016/j.bmcl.2013.11.039