(5,10,15,20-tetraphenylporphyrinato-κ4N)(trifluoromethylsulfonate)iron(III)

Base Information

Chemical Name:(5,10,15,20-tetraphenylporphyrinato-κ4N)(trifluoromethylsulfonate)iron(III)
CAS No.:70936-35-5
Molecular Formula:C₄₅H₂₈F₃FeN₄O₃S
Molecular Weight:817.651
Hs Code.:

Synonyms:(5,10,15,20-tetraphenylporphyrinato-κ4N)(trifluoromethylsulfonate)iron(III)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5,10,15,20-tetraphenylporphyrinato-κ4N)(trifluoromethylsulfonate)iron(III)

Chemical Property:

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Technology Process of (5,10,15,20-tetraphenylporphyrinato-κ4N)(trifluoromethylsulfonate)iron(III)

There total 4 articles about (5,10,15,20-tetraphenylporphyrinato-κ4N)(trifluoromethylsulfonate)iron(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 16456-81-8,170645-84-8
meso-tetraphenylporphyrin iron(III) chloride

: 2923-28-6
silver trifluoromethanesulfonate

: 70936-35-5
(5,10,15,20-tetraphenylporphyrinato-κ4N)(trifluoromethylsulfonate)iron(III)

Guidance literature:: In tetrahydrofuran; byproducts: AgCl; Ar-atmosphere; stoich. amts., refluxing (30 min); filtration off of AgCl, crystn. on heptane addn. (refrigerator, overnight), filtration, washing (toluene), drying (vac., over P2O5, room temp., overnight), recrystn. (toluene/heptane); elem. anal.;

Reference yield:

: 1493-13-6
trifluorormethanesulfonic acid

: C₄₈H₃₇FeN₆O₂*0.74CH₂Cl₂

: 70936-35-5
(5,10,15,20-tetraphenylporphyrinato-κ4N)(trifluoromethylsulfonate)iron(III)

: 917-95-3
t-butylnitrite

: 10024-97-2
dinitrogen monoxide

Guidance literature:: With 1-methyl-1H-imidazole; In chloroform-d1; at 20 ℃; for 1h; Sealed tube; Darkness; Inert atmosphere;
DOI:10.1039/c5dt03074a

Reference yield:

: 12582-61-5
((5,10,15,20-tetraphenylporphyrinato)iron(III))2O

: 1493-13-6
trifluorormethanesulfonic acid

: 70936-35-5
(5,10,15,20-tetraphenylporphyrinato-κ4N)(trifluoromethylsulfonate)iron(III)

Guidance literature:: In dichloromethane; water; stirred for 1 h with aq. HSO3CF3; layers sepd., crystn. by adding heptane, elem. anal.;
DOI:10.1021/ic00132a023