ethyl 2-({[(2'-cyan-1,1'-biphenyl-4-yl)methyl]amino}carbonyl)pyrrolidine-1-carboxylate

Base Information

Chemical Name:ethyl 2-({[(2'-cyan-1,1'-biphenyl-4-yl)methyl]amino}carbonyl)pyrrolidine-1-carboxylate
CAS No.:1334672-20-6
Molecular Formula:C₂₂H₂₃N₃O₃
Molecular Weight:377.443
Hs Code.:

Synonyms:ethyl 2-({[(2'-cyan-1,1'-biphenyl-4-yl)methyl]amino}carbonyl)pyrrolidine-1-carboxylate

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Chemical Property of ethyl 2-({[(2'-cyan-1,1'-biphenyl-4-yl)methyl]amino}carbonyl)pyrrolidine-1-carboxylate

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Technology Process of ethyl 2-({[(2'-cyan-1,1'-biphenyl-4-yl)methyl]amino}carbonyl)pyrrolidine-1-carboxylate

There total 2 articles about ethyl 2-({[(2'-cyan-1,1'-biphenyl-4-yl)methyl]amino}carbonyl)pyrrolidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 956243-28-0
C₁₉H₁₉N₃O

: 1609-47-8
diethyl dicarbonate

: 1334672-20-6
ethyl 2-({[(2'-cyan-1,1'-biphenyl-4-yl)methyl]amino}carbonyl)pyrrolidine-1-carboxylate

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; at 0 - 20 ℃; for 4h;
DOI:10.1002/ardp.201000296

Reference yield:

: 956242-65-2
C₂₄H₂₇N₃O₃

: 1334672-20-6
ethyl 2-({[(2'-cyan-1,1'-biphenyl-4-yl)methyl]amino}carbonyl)pyrrolidine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen bromide / ethyl acetate / 20 °C

2: sodium hydroxide / tetrahydrofuran / 4 h / 0 - 20 °C

With hydrogen bromide; sodium hydroxide; In tetrahydrofuran; ethyl acetate;
DOI:10.1002/ardp.201000296