(2,6-bis(3-tert-butyl-5-methyl-2-oxybenzyl)-4-methyl-anisole)Zr(CH₂Ph)2

Base Information

• Chemical Name: (2,6-bis(3-tert-butyl-5-methyl-2-oxybenzyl)-4-methyl-anisole)Zr(CH₂Ph)2
• CAS No.: 873583-64-3
• Molecular Formula: C₄₆H₅₄O₃Zr
• Molecular Weight: 746.157

Synonyms:(2,6-bis(3-tert-butyl-5-methyl-2-oxybenzyl)-4-methyl-anisole)Zr(CH₂Ph)2

Chemical Property of (2,6-bis(3-tert-butyl-5-methyl-2-oxybenzyl)-4-methyl-anisole)Zr(CH₂Ph)2

Chemical Property:

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Technology Process of (2,6-bis(3-tert-butyl-5-methyl-2-oxybenzyl)-4-methyl-anisole)Zr(CH₂Ph)2

There total 1 articles about (2,6-bis(3-tert-butyl-5-methyl-2-oxybenzyl)-4-methyl-anisole)Zr(CH₂Ph)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

((2,6-bis(3-tert-butyl-5-methyl-2-oxybenzyl)-4-methyl-anisole)ZrCl)2(μ-OTf)2 + benzylmagnesium chloride (6921-34-2) → (2,6-bis(3-tert-butyl-5-methyl-2-oxybenzyl)-4-methyl-anisole)Zr(CH2Ph)2 (873583-64-3)

Guidance literature:

In tetrahydrofuran; toluene; addn. of 4 equiv. of magnesium compd. to zirconium compd.;

DOI:10.1021/ja0567079

Reference yield: 99.0%

(2,6-bis(3-tert-butyl-5-methyl-2-oxybenzyl)-4-methyl-anisole)Zr(CH2Ph)2 (873583-64-3) + hydrogen (1333-74-0) → (2,6-bis(3-tert-butyl-5-methyl-2-oxybenzyl)-4-methyl-anisole)Zr(CH2Ph)2 (873583-65-4)

Guidance literature:

In toluene; byproducts: toluene; treating zirconium compd. with H2 under 1 atm. in toluene at room temp.;

DOI:10.1021/ja0567079

upstream raw materials:

benzylmagnesium chloride

Downstream raw materials:

(2,6-bis(3-tert-butyl-5-methyl-2-oxybenzyl)-4-methyl-anisole)Zr(CH₂Ph)2

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