4-[3-(1,3-DIOXO-1,3-DIHYDRO-2H-ISOINDOL-2-YL)PROPOXY]BENZENECARBONITRILE

Base Information

• Chemical Name: 4-[3-(1,3-DIOXO-1,3-DIHYDRO-2H-ISOINDOL-2-YL)PROPOXY]BENZENECARBONITRILE
• CAS No.: 313476-81-2
• Molecular Formula: C₁₈H₁₄N₂O₃
• Molecular Weight: 306.321
• Mol file: 313476-81-2.mol

Synonyms:4-[3-(1,3-Dioxo-1,3-dihydro-2H-isoindol-2-yl)propoxy]benzonitrile

Chemical Property of 4-[3-(1,3-DIOXO-1,3-DIHYDRO-2H-ISOINDOL-2-YL)PROPOXY]BENZENECARBONITRILE

Chemical Property:

• Melting Point: 105-107°

Purity/Quality:

98%min ^*data from raw suppliers

4-[3-(1,3-Dioxo-1,3-dihydro-2H-isoindol-2-yl)-propoxy]benzenecarbonitrile >95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-[3-(1,3-DIOXO-1,3-DIHYDRO-2H-ISOINDOL-2-YL)PROPOXY]BENZENECARBONITRILE

There total 2 articles about 4-[3-(1,3-DIOXO-1,3-DIHYDRO-2H-ISOINDOL-2-YL)PROPOXY]BENZENECARBONITRILE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-(3-Bromopropoxy)benzonitrile (37136-86-0) + potassium phtalimide (1074-82-4) → 4-[3-(1,3-Dioxo-1,3-dihydro-2H-isoindol-2-yl)propoxy]benzonitrile (313476-81-2)

Guidance literature:

In DMF (N,N-dimethyl-formamide); at 95 ℃; for 4h;

Reference yield:

→ 4-[3-(1,3-Dioxo-1,3-dihydro-2H-isoindol-2-yl)propoxy]benzonitrile (313476-81-2)

Guidance literature:

Reference yield: 41.0%

4-[3-(1,3-Dioxo-1,3-dihydro-2H-isoindol-2-yl)propoxy]benzonitrile (313476-81-2) → 4-(3-aminopropoxy)benzonitrile (116753-55-0)

Guidance literature:

4-[3-(1,3-Dioxo-1,3-dihydro-2H-isoindol-2-yl)propoxy]benzonitrile; With hydrazine; In methanol; water; for 1h; Heating / reflux;

With hydrogenchloride; water; for 1.5h;

upstream raw materials:

4-(3-Bromopropoxy)benzonitrile

potassium phtalimide

Downstream raw materials:

4-(3-aminopropoxy)benzonitrile

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