carbonic acid 2-(2,3-dihydroxy-propyl)-cyclohex-2-enyl ester 2,2,2-trichloro-ethyl ester

Base Information

Chemical Name:carbonic acid 2-(2,3-dihydroxy-propyl)-cyclohex-2-enyl ester 2,2,2-trichloro-ethyl ester
CAS No.:869369-31-3
Molecular Formula:C₁₂H₁₇Cl₃O₅
Molecular Weight:347.623
Hs Code.:

Synonyms:carbonic acid 2-(2,3-dihydroxy-propyl)-cyclohex-2-enyl ester 2,2,2-trichloro-ethyl ester

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Chemical Property of carbonic acid 2-(2,3-dihydroxy-propyl)-cyclohex-2-enyl ester 2,2,2-trichloro-ethyl ester

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Technology Process of carbonic acid 2-(2,3-dihydroxy-propyl)-cyclohex-2-enyl ester 2,2,2-trichloro-ethyl ester

There total 3 articles about carbonic acid 2-(2,3-dihydroxy-propyl)-cyclohex-2-enyl ester 2,2,2-trichloro-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 869369-04-0
carbonic acid 2-allyl-cyclohex-2-enyl ester 2,2,2-trichloro-ethyl ester

: 869369-31-3
carbonic acid 2-(2,3-dihydroxy-propyl)-cyclohex-2-enyl ester 2,2,2-trichloro-ethyl ester

Guidance literature:: With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1021/ja054449+

Reference yield:

: 38019-50-0
2-allyl-cyclohex-2-enone

: 869369-31-3
carbonic acid 2-(2,3-dihydroxy-propyl)-cyclohex-2-enyl ester 2,2,2-trichloro-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / NaBH₄; CeCl₃ / methanol; CH₂Cl₂ / 1 h / 0 °C

2: 89 percent / 4-N,N-dimethylaminopyridine; pyridine / CH₂Cl₂

3: 81 percent / N-methylmorpholine N-oxide; OsO₄ / CH₂Cl₂ / 4 h / 20 °C

With pyridine; dmap; sodium tetrahydroborate; osmium(VIII) oxide; cerium(III) chloride; 4-methylmorpholine N-oxide; In methanol; dichloromethane; 1: Luche reduction;
DOI:10.1021/ja054449+

Reference yield:

: 176649-68-6
2-(prop-2'-enyl)-cyclohex-2-en-1-ol

: 869369-31-3
carbonic acid 2-(2,3-dihydroxy-propyl)-cyclohex-2-enyl ester 2,2,2-trichloro-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / 4-N,N-dimethylaminopyridine; pyridine / CH₂Cl₂

2: 81 percent / N-methylmorpholine N-oxide; OsO₄ / CH₂Cl₂ / 4 h / 20 °C

With pyridine; dmap; osmium(VIII) oxide; 4-methylmorpholine N-oxide; In dichloromethane;
DOI:10.1021/ja054449+