carbonic acid 2-allyl-cyclohex-2-enyl ester 2,2,2-trichloro-ethyl ester

Base Information

• Chemical Name: carbonic acid 2-allyl-cyclohex-2-enyl ester 2,2,2-trichloro-ethyl ester
• CAS No.: 869369-04-0
• Molecular Formula: C₁₂H₁₅Cl₃O₃
• Molecular Weight: 313.608

Synonyms:carbonic acid 2-allyl-cyclohex-2-enyl ester 2,2,2-trichloro-ethyl ester

Chemical Property of carbonic acid 2-allyl-cyclohex-2-enyl ester 2,2,2-trichloro-ethyl ester

Chemical Property:

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Technology Process of carbonic acid 2-allyl-cyclohex-2-enyl ester 2,2,2-trichloro-ethyl ester

There total 2 articles about carbonic acid 2-allyl-cyclohex-2-enyl ester 2,2,2-trichloro-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

2-(prop-2'-enyl)-cyclohex-2-en-1-ol (176649-68-6) + 2,2,2-Trichloroethyl chloroformate (17341-93-4) → carbonic acid 2-allyl-cyclohex-2-enyl ester 2,2,2-trichloro-ethyl ester (869369-04-0)

Guidance literature:

With pyridine; dmap; In dichloromethane;

DOI:10.1021/ja054449+

Reference yield:

2-allyl-cyclohex-2-enone (38019-50-0) → carbonic acid 2-allyl-cyclohex-2-enyl ester 2,2,2-trichloro-ethyl ester (869369-04-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 92 percent / NaBH₄; CeCl₃ / methanol; CH₂Cl₂ / 1 h / 0 °C

2: 89 percent / 4-N,N-dimethylaminopyridine; pyridine / CH₂Cl₂

With pyridine; dmap; sodium tetrahydroborate; cerium(III) chloride; In methanol; dichloromethane; 1: Luche reduction;

DOI:10.1021/ja054449+

Reference yield: 81.0%

carbonic acid 2-allyl-cyclohex-2-enyl ester 2,2,2-trichloro-ethyl ester (869369-04-0) → carbonic acid 2-(2,3-dihydroxy-propyl)-cyclohex-2-enyl ester 2,2,2-trichloro-ethyl ester (869369-31-3)

Guidance literature:

With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In dichloromethane; at 20 ℃; for 4h;

DOI:10.1021/ja054449+

upstream raw materials:

2-(prop-2'-enyl)-cyclohex-2-en-1-ol

2,2,2-Trichloroethyl chloroformate

2-allyl-cyclohex-2-enone

Downstream raw materials:

carbonic acid 2-(2,3-dihydroxy-propyl)-cyclohex-2-enyl ester 2,2,2-trichloro-ethyl ester

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