2-amino-2-deoxy-1,3,4-tri-O-dodecanoyl-β-D-glucopyranose 6-(diphenyl phosphate) hydrochloride

Base Information

Chemical Name:2-amino-2-deoxy-1,3,4-tri-O-dodecanoyl-β-D-glucopyranose 6-(diphenyl phosphate) hydrochloride
CAS No.:81347-87-7
Molecular Formula:C₅₄H₈₈NO₁₁P*ClH
Molecular Weight:994.728
Hs Code.:

Synonyms:2-amino-2-deoxy-1,3,4-tri-O-dodecanoyl-β-D-glucopyranose 6-(diphenyl phosphate) hydrochloride

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Chemical Property of 2-amino-2-deoxy-1,3,4-tri-O-dodecanoyl-β-D-glucopyranose 6-(diphenyl phosphate) hydrochloride

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Technology Process of 2-amino-2-deoxy-1,3,4-tri-O-dodecanoyl-β-D-glucopyranose 6-(diphenyl phosphate) hydrochloride

There total 4 articles about 2-amino-2-deoxy-1,3,4-tri-O-dodecanoyl-β-D-glucopyranose 6-(diphenyl phosphate) hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 81347-86-6
2-deoxy-1,3,4-tri-O-dodecanoyl-2-(4-methoxybenzylidene)amino-β-D-glucopyranose 6-(diphenyl phosphate)

: 81347-87-7
2-amino-2-deoxy-1,3,4-tri-O-dodecanoyl-β-D-glucopyranose 6-(diphenyl phosphate) hydrochloride

Guidance literature:: With hydrogenchloride; In water; acetone; 1.) reflux, 1 min, 2.) 20 h, 5 deg C;
DOI:10.1016/S0008-6215(00)81016-2

Reference yield:

: 112-16-3
n-dodecanoyl chloride

: 81347-87-7
2-amino-2-deoxy-1,3,4-tri-O-dodecanoyl-β-D-glucopyranose 6-(diphenyl phosphate) hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) pyridine, 2.) pyridine / 1.) -5 deg C, 12 h, 2.) CHCl₃, 1.5 h, 70 deg C

2: 78 percent / 6M hydrochoric acid / acetone; H₂O / 1.) reflux, 1 min, 2.) 20 h, 5 deg C

With pyridine; hydrogenchloride; In water; acetone;
DOI:10.1016/S0008-6215(00)81016-2

Reference yield:

: 35946-64-6
2-deoxy-2-(4-methoxybenzylidene)amino-D-glucose

: 81347-87-7
2-amino-2-deoxy-1,3,4-tri-O-dodecanoyl-β-D-glucopyranose 6-(diphenyl phosphate) hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) pyridine, 2.) pyridine / 1.) -5 deg C, 12 h, 2.) CHCl₃, 1.5 h, 70 deg C

2: 78 percent / 6M hydrochoric acid / acetone; H₂O / 1.) reflux, 1 min, 2.) 20 h, 5 deg C

With pyridine; hydrogenchloride; In water; acetone;
DOI:10.1016/S0008-6215(00)81016-2