2-deoxy-1,3,4-tri-O-dodecanoyl-2-(4-methoxybenzylidene)amino-β-D-glucopyranose 6-(diphenyl phosphate)

Base Information

Chemical Name:2-deoxy-1,3,4-tri-O-dodecanoyl-2-(4-methoxybenzylidene)amino-β-D-glucopyranose 6-(diphenyl phosphate)
CAS No.:81347-86-6
Molecular Formula:C₆₂H₉₄NO₁₂P
Molecular Weight:1076.4
Hs Code.:

Synonyms:2-deoxy-1,3,4-tri-O-dodecanoyl-2-(4-methoxybenzylidene)amino-β-D-glucopyranose 6-(diphenyl phosphate)

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Chemical Property of 2-deoxy-1,3,4-tri-O-dodecanoyl-2-(4-methoxybenzylidene)amino-β-D-glucopyranose 6-(diphenyl phosphate)

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Technology Process of 2-deoxy-1,3,4-tri-O-dodecanoyl-2-(4-methoxybenzylidene)amino-β-D-glucopyranose 6-(diphenyl phosphate)

There total 1 articles about 2-deoxy-1,3,4-tri-O-dodecanoyl-2-(4-methoxybenzylidene)amino-β-D-glucopyranose 6-(diphenyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112-16-3
n-dodecanoyl chloride

: 35946-64-6
2-deoxy-2-(4-methoxybenzylidene)amino-D-glucose

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 81347-86-6
2-deoxy-1,3,4-tri-O-dodecanoyl-2-(4-methoxybenzylidene)amino-β-D-glucopyranose 6-(diphenyl phosphate)

Guidance literature:: With pyridine; Yield given. Multistep reaction; 1.) -5 deg C, 12 h, 2.) CHCl₃, 1.5 h, 70 deg C;
DOI:10.1016/S0008-6215(00)81016-2

Reference yield: 78.0%

: 81347-86-6
2-deoxy-1,3,4-tri-O-dodecanoyl-2-(4-methoxybenzylidene)amino-β-D-glucopyranose 6-(diphenyl phosphate)

: 81347-87-7
2-amino-2-deoxy-1,3,4-tri-O-dodecanoyl-β-D-glucopyranose 6-(diphenyl phosphate) hydrochloride

Guidance literature:: With hydrogenchloride; In water; acetone; 1.) reflux, 1 min, 2.) 20 h, 5 deg C;
DOI:10.1016/S0008-6215(00)81016-2

Reference yield:

: 81347-86-6
2-deoxy-1,3,4-tri-O-dodecanoyl-2-(4-methoxybenzylidene)amino-β-D-glucopyranose 6-(diphenyl phosphate)

: 81347-88-8
2-acetamido-2-deoxy-1,3,4-tri-O-dodecanoyl-β-D-glucopyranose 6-(diphenyl phosphate)

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / 6M hydrochoric acid / acetone; H₂O / 1.) reflux, 1 min, 2.) 20 h, 5 deg C

2: 90 percent / pyridine / 20 h / 25 °C

With pyridine; hydrogenchloride; In water; acetone;
DOI:10.1016/S0008-6215(00)81016-2