tert-Butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-benzyloxyvalerate

Base Information

Chemical Name:tert-Butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-benzyloxyvalerate
CAS No.:1404378-83-1
Molecular Formula:C₂₇H₃₃NO₆
Molecular Weight:467.562
Hs Code.:

Synonyms:tert-Butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-benzyloxyvalerate

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Chemical Property of tert-Butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-benzyloxyvalerate

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Technology Process of tert-Butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-benzyloxyvalerate

There total 2 articles about tert-Butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-benzyloxyvalerate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 169897-87-4
[4S]-4-benzyl-3-(4-benzyloxy-1-butanoyl)-2-oxazolidinone

: 1404378-83-1
tert-Butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-benzyloxyvalerate

Guidance literature:: [4S]-4-benzyl-3-(4-benzyloxy-1-butanoyl)-2-oxazolidinone; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 - -50 ℃;

bromoacetic acid tert-butyl ester; In tetrahydrofuran; at -78 - -15 ℃;

With N,N,N'-triethylethanediamine; In tetrahydrofuran;

Reference yield:

: 10385-30-5
4-(benzyloxy)butanoic acid

: 90719-32-7
(S)-4-Benzyl-2-oxazolidinone

: 1404378-83-1
tert-Butyl 3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)-5-benzyloxyvalerate

Guidance literature:: Multi-step reaction with 2 steps

1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / chloroform / 20 °C / Cooling with ice

2.1: sodium hexamethyldisilazane / tetrahydrofuran / -78 - -50 °C

2.2: -78 - -15 °C

With dmap; sodium hexamethyldisilazane; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; chloroform;