1,6-di-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-pivaloyl-D-glucopyranose

Base Information

Chemical Name:1,6-di-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-pivaloyl-D-glucopyranose
CAS No.:849101-38-8
Molecular Formula:C₂₂H₂₉N₃O₈
Molecular Weight:463.488
Hs Code.:

Synonyms:1,6-di-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-pivaloyl-D-glucopyranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,6-di-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-pivaloyl-D-glucopyranose

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Technology Process of 1,6-di-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-pivaloyl-D-glucopyranose

There total 1 articles about 1,6-di-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-pivaloyl-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 3282-30-2
pivaloyl chloride

: 1,6-di-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α,β-D-glucopyranose

: 849101-38-8
1,6-di-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-pivaloyl-D-glucopyranose

Guidance literature:: With pyridine; In N,N-dimethyl-formamide; at 45 ℃; for 48h;
DOI:10.1016/j.carres.2004.11.029

Reference yield: 80.0%

: 849101-38-8
1,6-di-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-pivaloyl-D-glucopyranose

: 6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-pivaloyl-D-glucopyranose

Guidance literature:: With hydrazinium monoacetate; In N,N-dimethyl-formamide; at 20 ℃; for 2.5h;
DOI:10.1016/j.carres.2004.11.029

Reference yield:

: 849101-38-8
1,6-di-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-pivaloyl-D-glucopyranose

: 849101-40-2
6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-pivaloyl-α-D-glucopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / N₂H₄*HOAc / dimethylformamide / 2.5 h / 20 °C

2: 58 percent / Cs₂CO₃ / CH₂Cl₂ / 1 h / 0 °C

With hydrazinium monoacetate; caesium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2004.11.029