1-(3,4-dimethoxyphenyl)-t-4--N-methylamino>-r-1-cyclohexanecarbonitrile

Base Information

Chemical Name:1-(3,4-dimethoxyphenyl)-t-4--N-methylamino>-r-1-cyclohexanecarbonitrile
CAS No.:133648-51-8
Molecular Formula:C₂₆H₃₄N₂O₄
Molecular Weight:438.567
Hs Code.:

1-(3,4-dimethoxyphenyl)-t-4-<N-<2-(3,4-dimethoxyphenyl)ethyl>-N-methylamino>-r-1-cyclohexanecarbonitrile

Synonyms:1-(3,4-dimethoxyphenyl)-t-4--N-methylamino>-r-1-cyclohexanecarbonitrile

Suppliers and Price of 1-(3,4-dimethoxyphenyl)-t-4--N-methylamino>-r-1-cyclohexanecarbonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-(3,4-dimethoxyphenyl)-t-4--N-methylamino>-r-1-cyclohexanecarbonitrile

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(3,4-dimethoxyphenyl)-t-4--N-methylamino>-r-1-cyclohexanecarbonitrile

There total 6 articles about 1-(3,4-dimethoxyphenyl)-t-4--N-methylamino>-r-1-cyclohexanecarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 40173-90-8
3,4-dimethoxyphenethyl bromide

: 133648-70-1
1-(3,4-dimethoxyphenyl)-t-4-(methylamino)-r-1-cyclohexanecarbonitrile

: 133648-51-8
1-(3,4-dimethoxyphenyl)-t-4--N-methylamino>-r-1-cyclohexanecarbonitrile

Guidance literature:: With potassium carbonate; In acetonitrile; for 44h; Heating;
DOI:10.1021/jm00111a043

Reference yield:

: 51533-65-4
4-(3,4-dimethoxyphenyl)-4-cyanocyclohexanone

: 133648-51-8
1-(3,4-dimethoxyphenyl)-t-4--N-methylamino>-r-1-cyclohexanecarbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: p-toluenesulfonic acid monohydrate / 45 h / Heating

2: NaBH₄ / methanol / 2 h / Heating

3: 1.) 85percent HCOOH / 1.) ethanol, reflux, 1 h, 2.) ethanol, reflux, 5 h

With sodium tetrahydroborate; formic acid; toluene-4-sulfonic acid; In methanol;
DOI:10.1021/jm00111a043

Reference yield:

: 133648-53-0
methyl 5-cyano-5-(3,4-dimethoxyphenyl)-2-oxocyclohexanecarboxylate

: 133648-51-8
1-(3,4-dimethoxyphenyl)-t-4--N-methylamino>-r-1-cyclohexanecarbonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: 66 percent / acetic acid, 10percent sulfuric acid / 5 h / Heating

2: p-toluenesulfonic acid monohydrate / 45 h / Heating

3: NaBH₄ / methanol / 2 h / Heating

4: 1.) 85percent HCOOH / 1.) ethanol, reflux, 1 h, 2.) ethanol, reflux, 5 h

With sodium tetrahydroborate; formic acid; sulfuric acid; toluene-4-sulfonic acid; acetic acid; In methanol;
DOI:10.1021/jm00111a043