benzyloxy-[2-(tert-butyloxycarbonylamino)ethoxy]-(N,N-diisopropylamino)phosphine

Base Information

Chemical Name:benzyloxy-[2-(tert-butyloxycarbonylamino)ethoxy]-(N,N-diisopropylamino)phosphine
CAS No.:1023637-24-2
Molecular Formula:C₂₀H₃₅N₂O₄P
Molecular Weight:398.483
Hs Code.:

Synonyms:benzyloxy-[2-(tert-butyloxycarbonylamino)ethoxy]-(N,N-diisopropylamino)phosphine

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Chemical Property of benzyloxy-[2-(tert-butyloxycarbonylamino)ethoxy]-(N,N-diisopropylamino)phosphine

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Technology Process of benzyloxy-[2-(tert-butyloxycarbonylamino)ethoxy]-(N,N-diisopropylamino)phosphine

There total 1 articles about benzyloxy-[2-(tert-butyloxycarbonylamino)ethoxy]-(N,N-diisopropylamino)phosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 26690-80-2
2-(N-tert-butoxycarbonylamino)ethanol

: 108549-21-9
benzyl-N,N,N',N'-tetraisopropylphosphorodiamidite

: 1023637-24-2
benzyloxy-[2-(tert-butyloxycarbonylamino)ethoxy]-(N,N-diisopropylamino)phosphine

Guidance literature:: With 1H-tetrazole; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1039/b717564g

Reference yield: 89.0%

: 1023637-24-2
benzyloxy-[2-(tert-butyloxycarbonylamino)ethoxy]-(N,N-diisopropylamino)phosphine

: 2-(N-benzyloxycarbonyl)aminoethyl (2,3,4,6,7-penta-O-benzoyl-L-glycero-α-D-manno-heptopyranosyl)-(1->2)-(3,4,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranosyl)-(1->3)-[(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-(1->4)]-6,7-di-O-acetyl-2-O-benzyl-L-glycero-α-D-manno-heptopyranoside

: 2-(N-benzyloxycarbonyl)aminoethyl (2,3,4,6,7-penta-O-benzoyl-L-glycero-α-D-manno-heptopyranosyl)-(1->2)-(3,4,7-tri-O-acetyl-6-O-[benzyl-2-(tert-butyloxycarbonylaminoethyl)phosphono]-L-glycero-α-D-manno-heptopyranosyl)-(1->3)-[(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-(1->4)]-6,7-di-O-acetyl-2-O-benzyl-L-glycero-α-D-manno-heptopyranoside

Guidance literature:: benzyloxy-[2-(tert-butyloxycarbonylamino)ethoxy]-(N,N-diisopropylamino)phosphine; 2-(N-benzyloxycarbonyl)aminoethyl (2,3,4,6,7-penta-O-benzoyl-L-glycero-α-D-manno-heptopyranosyl)-(1->2)-(3,4,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranosyl)-(1->3)-[(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-(1->4)]-6,7-di-O-acetyl-2-O-benzyl-L-glycero-α-D-manno-heptopyranoside; With 1H-tetrazole; In dichloromethane; at 20 ℃; for 4h;

With 3-chloro-benzenecarboperoxoic acid; at 0 - 20 ℃;
DOI:10.1039/b717564g

Reference yield: 76.0%

: 1023637-24-2
benzyloxy-[2-(tert-butyloxycarbonylamino)ethoxy]-(N,N-diisopropylamino)phosphine

: 2-(benzyloxycarbonylamino)ethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranosyl-(1->2)-3,4,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranosyl-(1->3)-[2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->4)]-6,7-di-O-acetyl-2-O-benzyl-L-glycero-α-D-manno-heptopyranoside

: 2-(benzyloxycarbonylamino)ethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranosyl-(1->2)-3,4,7-tri-O-acetyl-6-O-[(benzyl)(2-(tert-butyloxycarbonylamino)ethyl)phosphono]-L-glycero-α-D-manno-heptopyranosyl-(1->3)-[2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->4)]-6,7-di-O-acetyl-2-O-benzyl-L-glycero-α-D-manno-heptopyranoside

Guidance literature:: benzyloxy-[2-(tert-butyloxycarbonylamino)ethoxy]-(N,N-diisopropylamino)phosphine; 2-(benzyloxycarbonylamino)ethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranosyl-(1->2)-3,4,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranosyl-(1->3)-[2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->4)]-6,7-di-O-acetyl-2-O-benzyl-L-glycero-α-D-manno-heptopyranoside; With 1H-tetrazole; In dichloromethane; for 2h;

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; for 0.25h;
DOI:10.1016/j.tetasy.2009.02.017