N,N-diisopropyl-P-phenyl-P-(2-(trimethylsilyl)phenyl)phosphinothioic amide

Base Information

Chemical Name:N,N-diisopropyl-P-phenyl-P-(2-(trimethylsilyl)phenyl)phosphinothioic amide
CAS No.:1388802-96-7
Molecular Formula:C₂₁H₃₂NPSSi
Molecular Weight:389.617
Hs Code.:

Synonyms:N,N-diisopropyl-P-phenyl-P-(2-(trimethylsilyl)phenyl)phosphinothioic amide

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Chemical Property of N,N-diisopropyl-P-phenyl-P-(2-(trimethylsilyl)phenyl)phosphinothioic amide

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Technology Process of N,N-diisopropyl-P-phenyl-P-(2-(trimethylsilyl)phenyl)phosphinothioic amide

There total 4 articles about N,N-diisopropyl-P-phenyl-P-(2-(trimethylsilyl)phenyl)phosphinothioic amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 75-77-4
chloro-trimethyl-silane

: N,N-diisopropyl-P,P-diphenylphosphinothioic amide

: 1388802-96-7
N,N-diisopropyl-P-phenyl-P-(2-(trimethylsilyl)phenyl)phosphinothioic amide

Guidance literature:: N,N-diisopropyl-P,P-diphenylphosphinothioic amide; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In diethyl ether; hexane; at 0 ℃; for 2h; Inert atmosphere;

chloro-trimethyl-silane; In diethyl ether; hexane; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/c2ob25395j

Reference yield:

: 22859-57-0
N,N-diisopropyl-1,1-diphenylphosphanamine

: 1388802-96-7
N,N-diisopropyl-P-phenyl-P-(2-(trimethylsilyl)phenyl)phosphinothioic amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfur / toluene / 12 h / 0 - 20 °C / Inert atmosphere

2.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / diethyl ether; hexane / 2 h / 0 °C / Inert atmosphere

2.2: 0.5 h / 0 °C / Inert atmosphere

With sulfur; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In diethyl ether; hexane; toluene;
DOI:10.1039/c2ob25395j

Reference yield:

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 1388802-96-7
N,N-diisopropyl-P-phenyl-P-(2-(trimethylsilyl)phenyl)phosphinothioic amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / toluene / 2 h / 120 °C

2.1: sulfur / toluene / 12 h / 0 - 20 °C / Inert atmosphere

3.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / diethyl ether; hexane / 2 h / 0 °C / Inert atmosphere

3.2: 0.5 h / 0 °C / Inert atmosphere

With sulfur; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; triethylamine; In diethyl ether; hexane; toluene;
DOI:10.1039/c2ob25395j