6-chloro-3-(4-chloroanilino)-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl chloride

Base Information

• Chemical Name: 6-chloro-3-(4-chloroanilino)-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl chloride
• CAS No.: 933466-73-0
• Molecular Formula: C₁₄H₇Cl₃N₂O₃S₂
• Molecular Weight: 421.712
• Mol file: 933466-73-0.mol

Synonyms:6-chloro-3-(4-chloroanilino)-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl chloride

Chemical Property of 6-chloro-3-(4-chloroanilino)-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6-chloro-3-(4-chloroanilino)-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl chloride

There total 1 articles about 6-chloro-3-(4-chloroanilino)-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

6-chloro-3-(4-chloro-phenylamino)-1,1-dioxo-1H-1λ6-benzo[1,4,2]dithiazine-7-carboxylic acid → 6-chloro-3-(4-chloroanilino)-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl chloride (933466-73-0)

Guidance literature:

With thionyl chloride; In benzene; for 16h; Heating;

DOI:10.1016/j.bmc.2007.01.052

Reference yield: 97.0%

6-chloro-3-(4-chloroanilino)-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl chloride (933466-73-0) → 6-chloro-3-(4-chlorophenylamino)-1,1-dioxo-1,4,2-benzodithiazine-7-carboxamide (933466-82-1)

Guidance literature:

With ammonia; In water; benzene; at 20 ℃; for 10h;

DOI:10.1016/j.bmc.2007.01.052

Reference yield: 96.0%

6-chloro-3-(4-chloroanilino)-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl chloride (933466-73-0) + ethanol (64-17-5) → ethyl 6-chloro-3-(4-chloroanilino)-1,1-dioxo-1,4,2-benzodithiazine-7-carboxylate (933466-77-4)

Guidance literature:

With triethylamine; Heating;

DOI:10.1016/j.bmc.2007.01.052

Downstream raw materials:

6-chloro-3-(4-chlorophenylamino)-1,1-dioxo-1,4,2-benzodithiazine-7-carboxamide

ethyl 6-chloro-3-(4-chloroanilino)-1,1-dioxo-1,4,2-benzodithiazine-7-carboxylate

6-chloro-3-(4-chlorophenylamino)-1,1-dioxo-1,4,2-benzodithiazine-7-carbonitrile