3'-O-bis(benzyl)phosphoryl-4-(tert-butyldiphenylsilyloxy)-3,4',5-trimethoxy-(Z)-stilbene

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Chemical Name:3'-O-bis(benzyl)phosphoryl-4-(tert-butyldiphenylsilyloxy)-3,4',5-trimethoxy-(Z)-stilbene
CAS No.:1207357-18-3
Molecular Formula:C₄₇H₄₉O₈PSi
Molecular Weight:800.961
Hs Code.:

Synonyms:3'-O-bis(benzyl)phosphoryl-4-(tert-butyldiphenylsilyloxy)-3,4',5-trimethoxy-(Z)-stilbene

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Chemical Property of 3'-O-bis(benzyl)phosphoryl-4-(tert-butyldiphenylsilyloxy)-3,4',5-trimethoxy-(Z)-stilbene

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Technology Process of 3'-O-bis(benzyl)phosphoryl-4-(tert-butyldiphenylsilyloxy)-3,4',5-trimethoxy-(Z)-stilbene

There total 2 articles about 3'-O-bis(benzyl)phosphoryl-4-(tert-butyldiphenylsilyloxy)-3,4',5-trimethoxy-(Z)-stilbene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 17176-77-1
Dibenzyl phosphite

: 1207357-16-1
4-(tert-butyldiphenylsilyloxy)-3'-hydroxy-3,4',5-trimethoxy-(Z)-stilbene

: 1207357-18-3
3'-O-bis(benzyl)phosphoryl-4-(tert-butyldiphenylsilyloxy)-3,4',5-trimethoxy-(Z)-stilbene

Guidance literature:: 4-(tert-butyldiphenylsilyloxy)-3'-hydroxy-3,4',5-trimethoxy-(Z)-stilbene; With tetrachloromethane; dmap; N-ethyl-N,N-diisopropylamine; In acetonitrile; at -10 ℃; for 0.183333h;

Dibenzyl phosphite; In acetonitrile; at -10 ℃; for 3.08333h;
DOI:10.1021/np9004486

Reference yield: 25.0%

: 3-O-bis(benzyl)phosphoryl-4-methoxybenzaldehyde

: 1207357-11-6
4-(tert-butyldiphenylsilyloxy)-3,5-dimethoxybenzyltriphenylphosphonium bromide

: 1207357-18-3
3'-O-bis(benzyl)phosphoryl-4-(tert-butyldiphenylsilyloxy)-3,4',5-trimethoxy-(Z)-stilbene

Guidance literature:: 4-(tert-butyldiphenylsilyloxy)-3,5-dimethoxybenzyltriphenylphosphonium bromide; With sodium hydride; In toluene; for 1h;

3-O-bis(benzyl)phosphoryl-4-methoxybenzaldehyde; In toluene; at 0 - 20 ℃; for 22h;
DOI:10.1021/np9004486