C₁₅H₃₀O₃Si

Base Information

Chemical Name:C₁₅H₃₀O₃Si
CAS No.:1464074-77-8
Molecular Formula:C₁₅H₃₀O₃Si
Molecular Weight:286.487
Hs Code.:

C<sub>15</sub>H<sub>30</sub>O<sub>3</sub>Si

Synonyms:C₁₅H₃₀O₃Si

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Chemical Property of C₁₅H₃₀O₃Si

Chemical Property:

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Technology Process of C₁₅H₃₀O₃Si

There total 3 articles about C₁₅H₃₀O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2031-62-1
diethoxymethylane

: 34737-39-8
2-butylcyclohex-2-en-1-one

: 1464074-77-8
C₁₅H₃₀O₃Si

Guidance literature:: diethoxymethylane; 2-butylcyclohex-2-en-1-one; With [(1,3-bis(2,4,6-trimethylphenyl)-imidazol-2-ylidene)Cu(dibenzoylmethanate)]; potassium tert-butylate; In toluene; at 0 ℃; for 1h; Schlenk technique; Inert atmosphere;

With water; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201404015

Reference yield:

: 930-68-7
cyclohexenone

: 1464074-77-8
C₁₅H₃₀O₃Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine; iodine / dichloromethane / 5 h / Schlenk technique; Inert atmosphere

2.1: zinc dibromide / tetrahydrofuran; hexane / -78 - 0 °C / Schlenk technique; Inert atmosphere

2.2: 3 h / 0 - 20 °C / Schlenk technique; Inert atmosphere

3.1: [(1,3-bis(2,4,6-trimethylphenyl)-imidazol-2-ylidene)Cu(dibenzoylmethanate)]; potassium tert-butylate / toluene / 1 h / 0 °C / Schlenk technique; Inert atmosphere

3.2: Inert atmosphere; Schlenk technique

With pyridine; [(1,3-bis(2,4,6-trimethylphenyl)-imidazol-2-ylidene)Cu(dibenzoylmethanate)]; potassium tert-butylate; iodine; zinc dibromide; In tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1002/chem.201404015

Reference yield:

: 33948-36-6
2-iodocyclohex-2-en-1-one

: 1464074-77-8
C₁₅H₃₀O₃Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: zinc dibromide / tetrahydrofuran; hexane / -78 - 0 °C / Schlenk technique; Inert atmosphere

1.2: 3 h / 0 - 20 °C / Schlenk technique; Inert atmosphere

2.1: [(1,3-bis(2,4,6-trimethylphenyl)-imidazol-2-ylidene)Cu(dibenzoylmethanate)]; potassium tert-butylate / toluene / 1 h / 0 °C / Schlenk technique; Inert atmosphere

2.2: Inert atmosphere; Schlenk technique

With [(1,3-bis(2,4,6-trimethylphenyl)-imidazol-2-ylidene)Cu(dibenzoylmethanate)]; potassium tert-butylate; zinc dibromide; In tetrahydrofuran; hexane; toluene;
DOI:10.1002/chem.201404015