4-methyl-N-(phenanthrene-9-ylmethylene)aniline

Base Information

Chemical Name:4-methyl-N-(phenanthrene-9-ylmethylene)aniline
CAS No.:1204704-27-7
Molecular Formula:C₂₂H₁₇N
Molecular Weight:295.384
Hs Code.:

Synonyms:4-methyl-N-(phenanthrene-9-ylmethylene)aniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methyl-N-(phenanthrene-9-ylmethylene)aniline

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Technology Process of 4-methyl-N-(phenanthrene-9-ylmethylene)aniline

There total 1 articles about 4-methyl-N-(phenanthrene-9-ylmethylene)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 106-49-0,12221-03-3
p-toluidine

: 4707-71-5
Phenanthrene-9-carboxaldehyde

: 1204704-27-7
4-methyl-N-(phenanthrene-9-ylmethylene)aniline

Guidance literature:: In methanol; at 120 ℃; Microwave irradiation; Sealed vessel; Inert atmosphere;
DOI:10.1016/j.jorganchem.2009.09.030

Reference yield: 66.0%

: 1204704-27-7
4-methyl-N-(phenanthrene-9-ylmethylene)aniline

: 1600-27-7
mercury(II) diacetate

: HgCl(4-methyl-N-(phenanthrene-9-ylmethylene)aniline)

Guidance literature:: With LiCl; In methanol; under N2; Schiff base and Hg acetate stirred (24 h) together in refluxing MeOH, mixt. cooled, LiCl in hot MeOH added under stirring; ppt. filtered, washed (Et2O), dried, solid extd. by hexane via G-4 soxlet frit, recrystn. (CHCl3-MeOH, 1:1);
DOI:10.1016/j.jorganchem.2009.09.030

Reference yield:

: 36309-68-9
p-methoxyphenyltellurium trichloride

: 1204704-27-7
4-methyl-N-(phenanthrene-9-ylmethylene)aniline

: 1204704-35-7
C₂₉H₂₃Cl₂NOTe

Guidance literature:: 4-methyl-N-(phenanthrene-9-ylmethylene)aniline; With mercury(II) diacetate; In methanol; for 24h; Reflux; Inert atmosphere;

With lithium chloride; In methanol; Inert atmosphere; Heating;

p-methoxyphenyltellurium trichloride; In chloroform; Reflux; Inert atmosphere;
DOI:10.1016/j.jorganchem.2009.09.030