C₆₀H₆₁Cl₃N₄O₁₅S

Base Information

Chemical Name:C₆₀H₆₁Cl₃N₄O₁₅S
CAS No.:874758-69-7
Molecular Formula:C₆₀H₆₁Cl₃N₄O₁₅S
Molecular Weight:1216.59
Hs Code.:

C<sub>60</sub>H<sub>61</sub>Cl<sub>3</sub>N<sub>4</sub>O<sub>15</sub>S

Synonyms:C₆₀H₆₁Cl₃N₄O₁₅S

Suppliers and Price of C₆₀H₆₁Cl₃N₄O₁₅S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆₀H₆₁Cl₃N₄O₁₅S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆₀H₆₁Cl₃N₄O₁₅S

There total 24 articles about C₆₀H₆₁Cl₃N₄O₁₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 874758-68-6
C₃₂H₃₅N₃O₉

: (S)-N-Troc-S-tris(4-methoxyphenyl)methane cystein

: 874758-69-7
C₆₀H₆₁Cl₃N₄O₁₅S

Guidance literature:: C₃₂H₃₅N₃O₉; (S)-N-Troc-S-tris(4-methoxyphenyl)methane cystein; With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 1h;

With sodium hydrogencarbonate; In dichloromethane; water;

Reference yield:

: 874758-51-7
ethyl 2-bromo-2-(6-(methoxymethoxy)-7-methylbenzo[d][1,3]dioxol-4-yl)acetate

: 874758-69-7
C₆₀H₆₁Cl₃N₄O₁₅S

Guidance literature:: Multi-step reaction with 12 steps

1: 68 percent / triethylamine / acetonitrile / 14 h / 0 °C

2: 97 percent / imidazole / dimethylformamide / 3 h / 23 °C

3: 94 percent / K₂CO₃; MeOH / 2 h / 23 °C

4: Dess-Martin periodinane / CH₂Cl₂ / 0.33 h / 23 °C

5: 1.26 g / ZnCl₂ / CH₂Cl₂; tetrahydrofuran / 0.17 h / 23 °C

6: 80 percent / LiBH₄ / tetrahydrofuran; methanol / 10 h / 0 °C

7: 92 percent / pyridine; DMAP / CH₂Cl₂ / 0.5 h / 23 °C

8: 91 percent / aq. HF / acetonitrile / 2 h / 23 °C

9: 93 percent / Dess-Martin periodinane / CH₂Cl₂ / 0.33 h / 20 °C

10: 95 percent / CF₃COOH / CH₂Cl₂ / 0.5 h / 23 °C

11: 96 percent / K₂CO₃; MeOH / 1 h / 20 °C

12: 95 percent / DMAP; EDCl / CH₂Cl₂ / 1 h / 20 °C

With pyridine; 1H-imidazole; methanol; dmap; lithium borohydride; hydrogen fluoride; potassium carbonate; Dess-Martin periodane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; zinc(II) chloride; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 4: Dess-Martin oxidation / 5: Strecker reaction / 9: Dess-Martin oxidation / 10: Pomerantz-Frisch-type cyclization;
DOI:10.1021/ja0571794

Reference yield:

: 874758-53-9
hydroxy-(7-hydroxy-6-methoxymethoxy-benzo[1,3]dioxol-4-yl)-acetic acid ethyl ester

: 874758-69-7
C₆₀H₆₁Cl₃N₄O₁₅S

Guidance literature:: Multi-step reaction with 15 steps

1: 95 percent / K₂CO₃ / dimethylformamide / 1 h / 23 °C

2: 93 percent / K₃PO₄; Pd(PPh₃)4 / dioxane / 4 h / 100 °C

3: 91 percent / benzotriazole; thionyl bromide / CH₂Cl₂ / 0.33 h / 20 °C

4: 68 percent / triethylamine / acetonitrile / 14 h / 0 °C

5: 97 percent / imidazole / dimethylformamide / 3 h / 23 °C

6: 94 percent / K₂CO₃; MeOH / 2 h / 23 °C

7: Dess-Martin periodinane / CH₂Cl₂ / 0.33 h / 23 °C

8: 1.26 g / ZnCl₂ / CH₂Cl₂; tetrahydrofuran / 0.17 h / 23 °C

9: 80 percent / LiBH₄ / tetrahydrofuran; methanol / 10 h / 0 °C

10: 92 percent / pyridine; DMAP / CH₂Cl₂ / 0.5 h / 23 °C

11: 91 percent / aq. HF / acetonitrile / 2 h / 23 °C

12: 93 percent / Dess-Martin periodinane / CH₂Cl₂ / 0.33 h / 20 °C

13: 95 percent / CF₃COOH / CH₂Cl₂ / 0.5 h / 23 °C

14: 96 percent / K₂CO₃; MeOH / 1 h / 20 °C

15: 95 percent / DMAP; EDCl / CH₂Cl₂ / 1 h / 20 °C

With pyridine; 1H-imidazole; methanol; dmap; 1,2,3-Benzotriazole; potassium phosphate; lithium borohydride; sulfurous dibromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydrogen fluoride; potassium carbonate; Dess-Martin periodane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; zinc(II) chloride; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 2: Suzuki-Miyaura cross-coupling reaction / 7: Dess-Martin oxidation / 8: Strecker reaction / 12: Dess-Martin oxidation / 13: Pomerantz-Frisch-type cyclization;
DOI:10.1021/ja0571794