1,4-anhydro-2-O-(p-methoxybenzoyl)-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-4-thio-D-ribitol

Base Information

Chemical Name:1,4-anhydro-2-O-(p-methoxybenzoyl)-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-4-thio-D-ribitol
CAS No.:658052-48-3
Molecular Formula:C₂₅H₄₂O₆SSi₂
Molecular Weight:526.842
Hs Code.:

Synonyms:1,4-anhydro-2-O-(p-methoxybenzoyl)-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-4-thio-D-ribitol

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Chemical Property of 1,4-anhydro-2-O-(p-methoxybenzoyl)-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-4-thio-D-ribitol

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Technology Process of 1,4-anhydro-2-O-(p-methoxybenzoyl)-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-4-thio-D-ribitol

There total 1 articles about 1,4-anhydro-2-O-(p-methoxybenzoyl)-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-4-thio-D-ribitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 100-07-2
4-methoxy-benzoyl chloride

: 291758-11-7
1,4-anhydro-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-4-thio-D-ribitol

: 658052-48-3
1,4-anhydro-2-O-(p-methoxybenzoyl)-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-4-thio-D-ribitol

Guidance literature:: With pyridine; at 20 ℃; for 12h;
DOI:10.1039/b305644a DOI:10.3987/COM-07-11250

Reference yield: 82.0%

: 658052-48-3
1,4-anhydro-2-O-(p-methoxybenzoyl)-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-4-thio-D-ribitol

: 1,4-anhydro-2-O-(4-methoxybenzoyl)-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-4-thio-D-ribitol-1-oxide

Guidance literature:: With ozone; In dichloromethane; at -78 - 20 ℃;

Reference yield: 54.0%

: 87-42-3
6-chloropurine

: 658052-48-3
1,4-anhydro-2-O-(p-methoxybenzoyl)-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-4-thio-D-ribitol

: 1020656-76-1
6-chloro-9-[2-O-(p-methoxybenzoyl)-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-4-thio-β-L-lyxofuranos-4-yl]-9H-purine

Guidance literature:: 6-chloropurine; With trimethylsilyl trifluoromethanesulfonate; triethylamine; In dichloromethane; at 20 ℃; for 1h;

1,4-anhydro-2-O-(p-methoxybenzoyl)-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-4-thio-D-ribitol; With bis-[(trifluoroacetoxy)iodo]benzene; In dichloromethane; for 24h; Further stages.;
DOI:10.3987/COM-07-11250