[(S)-1-[({[((S)-1-{(S)-1-[N'-(3-Amino-propionyl)-hydrazinocarbonyl]-3-methyl-butylcarbamoyl}-2-phenyl-ethylcarbamoyl)-methyl]-carbamoyl}-methyl)-carbamoyl]-2-(4-hydroxy-phenyl)-ethyl]-carbamic acid tert-butyl ester; compound with acetic acid

Base Information

Chemical Name:[(S)-1-[({[((S)-1-{(S)-1-[N'-(3-Amino-propionyl)-hydrazinocarbonyl]-3-methyl-butylcarbamoyl}-2-phenyl-ethylcarbamoyl)-methyl]-carbamoyl}-methyl)-carbamoyl]-2-(4-hydroxy-phenyl)-ethyl]-carbamic acid tert-butyl ester; compound with acetic acid
CAS No.:103310-91-4
Molecular Formula:C₂H₄O₂*C₃₆H₅₂N₈O₉
Molecular Weight:800.91
Hs Code.:

[(S)-1-[({[((S)-1-{(S)-1-[N'-(3-Amino-propionyl)-hydrazinocarbonyl]-3-methyl-butylcarbamoyl}-2-phenyl-ethylcarbamoyl)-methyl]-carbamoyl}-methyl)-carbamoyl]-2-(4-hydroxy-phenyl)-ethyl]-carbamic acid tert-butyl ester; compound with acetic acid

Synonyms:[(S)-1-[({[((S)-1-{(S)-1-[N'-(3-Amino-propionyl)-hydrazinocarbonyl]-3-methyl-butylcarbamoyl}-2-phenyl-ethylcarbamoyl)-methyl]-carbamoyl}-methyl)-carbamoyl]-2-(4-hydroxy-phenyl)-ethyl]-carbamic acid tert-butyl ester; compound with acetic acid

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Chemical Property of [(S)-1-[({[((S)-1-{(S)-1-[N'-(3-Amino-propionyl)-hydrazinocarbonyl]-3-methyl-butylcarbamoyl}-2-phenyl-ethylcarbamoyl)-methyl]-carbamoyl}-methyl)-carbamoyl]-2-(4-hydroxy-phenyl)-ethyl]-carbamic acid tert-butyl ester; compound with acetic acid

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Technology Process of [(S)-1-[({[((S)-1-{(S)-1-[N'-(3-Amino-propionyl)-hydrazinocarbonyl]-3-methyl-butylcarbamoyl}-2-phenyl-ethylcarbamoyl)-methyl]-carbamoyl}-methyl)-carbamoyl]-2-(4-hydroxy-phenyl)-ethyl]-carbamic acid tert-butyl ester; compound with acetic acid

There total 3 articles about [(S)-1-[({[((S)-1-{(S)-1-[N'-(3-Amino-propionyl)-hydrazinocarbonyl]-3-methyl-butylcarbamoyl}-2-phenyl-ethylcarbamoyl)-methyl]-carbamoyl}-methyl)-carbamoyl]-2-(4-hydroxy-phenyl)-ethyl]-carbamic acid tert-butyl ester; compound with acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 84047-93-8
[(S)-1-[({[((S)-1-{(S)-1-[N'-(3-Benzyloxycarbonylamino-propionyl)-hydrazinocarbonyl]-3-methyl-butylcarbamoyl}-2-phenyl-ethylcarbamoyl)-methyl]-carbamoyl}-methyl)-carbamoyl]-2-(4-hydroxy-phenyl)-ethyl]-carbamic acid tert-butyl ester

: 103310-91-4
[(S)-1-[({[((S)-1-{(S)-1-[N'-(3-Amino-propionyl)-hydrazinocarbonyl]-3-methyl-butylcarbamoyl}-2-phenyl-ethylcarbamoyl)-methyl]-carbamoyl}-methyl)-carbamoyl]-2-(4-hydroxy-phenyl)-ethyl]-carbamic acid tert-butyl ester; compound with acetic acid

Guidance literature:: With hydrogen; acetic acid; palladium on activated charcoal; In methanol; for 3h;

Reference yield:

: 68835-86-9
Boc-L-Tyr-Gly-Gly-L-Phe-L-Leu-OMe

: 103310-91-4
[(S)-1-[({[((S)-1-{(S)-1-[N'-(3-Amino-propionyl)-hydrazinocarbonyl]-3-methyl-butylcarbamoyl}-2-phenyl-ethylcarbamoyl)-methyl]-carbamoyl}-methyl)-carbamoyl]-2-(4-hydroxy-phenyl)-ethyl]-carbamic acid tert-butyl ester; compound with acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 86.6 percent / 98percent hydrazine hydrate / dimethylformamide / 24 h

2: 1.) 1-hydroxybenzotriazole, 2.) dicyclohexylcarbodiimide / 1.) DMF, 0 deg C, 2.) DMF, 0 deg C, 1 h, r.t., 1 h

3: 75 percent / 50percent acetic acid, H₂ / Pd/C / methanol / 3 h

With hydrogen; benzotriazol-1-ol; hydrazine hydrate; acetic acid; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 84047-92-7
Boc-Tyr-Gly-Gly-Phe-Leu-NHNH₂

: 103310-91-4
[(S)-1-[({[((S)-1-{(S)-1-[N'-(3-Amino-propionyl)-hydrazinocarbonyl]-3-methyl-butylcarbamoyl}-2-phenyl-ethylcarbamoyl)-methyl]-carbamoyl}-methyl)-carbamoyl]-2-(4-hydroxy-phenyl)-ethyl]-carbamic acid tert-butyl ester; compound with acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 1-hydroxybenzotriazole, 2.) dicyclohexylcarbodiimide / 1.) DMF, 0 deg C, 2.) DMF, 0 deg C, 1 h, r.t., 1 h

2: 75 percent / 50percent acetic acid, H₂ / Pd/C / methanol / 3 h

With hydrogen; benzotriazol-1-ol; acetic acid; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol;