methyl 2,3,4,6-tetradeoxy-2,6-bis-(2,4-dinitrophenylamino)-α-D-erythro-hexopyranoside

Base Information

Chemical Name:methyl 2,3,4,6-tetradeoxy-2,6-bis-(2,4-dinitrophenylamino)-α-D-erythro-hexopyranoside
CAS No.:165804-49-9
Molecular Formula:C₁₉H₂₀N₆O₁₀
Molecular Weight:492.402
Hs Code.:

Synonyms:methyl 2,3,4,6-tetradeoxy-2,6-bis-(2,4-dinitrophenylamino)-α-D-erythro-hexopyranoside

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Chemical Property of methyl 2,3,4,6-tetradeoxy-2,6-bis-(2,4-dinitrophenylamino)-α-D-erythro-hexopyranoside

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Technology Process of methyl 2,3,4,6-tetradeoxy-2,6-bis-(2,4-dinitrophenylamino)-α-D-erythro-hexopyranoside

There total 12 articles about methyl 2,3,4,6-tetradeoxy-2,6-bis-(2,4-dinitrophenylamino)-α-D-erythro-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 165804-46-6
methyl 2,3,4,6-tetradeoxy-2-(2,4-dinitrophenylamino)-6-<<2,4-dinitrophenyl-(1R)-phenylethyl>amino>-α-D-erythro-hexopyranoside

: 165804-49-9
methyl 2,3,4,6-tetradeoxy-2,6-bis-(2,4-dinitrophenylamino)-α-D-erythro-hexopyranoside

Guidance literature:: In trifluoroacetic acid; at 65 ℃; for 0.166667h;

Reference yield: 68.0%

: 40269-08-7
methyl 2,6-diamino-2,3,4,6-tetradeoxy-α-D-erythro-hexopyranose

: 70-34-8,65727-75-5
2,4-Dinitrofluorobenzene

: 165804-49-9
methyl 2,3,4,6-tetradeoxy-2,6-bis-(2,4-dinitrophenylamino)-α-D-erythro-hexopyranoside

Guidance literature:: With sodium hydrogencarbonate;

Reference yield:

: 2-<(1R)-phenylethylaminomethyl>-3,4-dihydro-2H-pyran

: 165804-49-9
methyl 2,3,4,6-tetradeoxy-2,6-bis-(2,4-dinitrophenylamino)-α-D-erythro-hexopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 1 h / 0 °C

2: 1.) NOCl, 2.) 1,3,5-trimethylpyrazole / 1.) CH₂Cl₂, -78 deg C

3: 300 mg / MoO₃, NaBH₄ / methanol / 5 h / 0 °C

4: NaHCO₃

5: 94 percent / trifluoroacetic acid / 0.17 h / 65 °C

With 1,3,5-trimethyl-1H-pyrazole; sodium tetrahydroborate; sodium hydrogencarbonate; nitrosylchloride; molybdenum(VI) oxide; In pyridine; methanol; trifluoroacetic acid;