S-methyl O-[1-phenyl-2-(2,4,6-triisopropylbenzoyloxy)ethyl] dithiocarbonate

Base Information

Chemical Name:S-methyl O-[1-phenyl-2-(2,4,6-triisopropylbenzoyloxy)ethyl] dithiocarbonate
CAS No.:1133931-92-6
Molecular Formula:C₂₆H₃₄O₃S₂
Molecular Weight:458.686
Hs Code.:

Synonyms:S-methyl O-[1-phenyl-2-(2,4,6-triisopropylbenzoyloxy)ethyl] dithiocarbonate

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Chemical Property of S-methyl O-[1-phenyl-2-(2,4,6-triisopropylbenzoyloxy)ethyl] dithiocarbonate

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Technology Process of S-methyl O-[1-phenyl-2-(2,4,6-triisopropylbenzoyloxy)ethyl] dithiocarbonate

There total 1 articles about S-methyl O-[1-phenyl-2-(2,4,6-triisopropylbenzoyloxy)ethyl] dithiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 75-15-0,12122-00-8
carbon disulfide

: 63846-79-7
(tributylstannyl)methyl 2,4,6-triisopropylbenzoate

: 100-52-7
benzaldehyde

: 74-88-4
methyl iodide

: 1133931-92-6
S-methyl O-[1-phenyl-2-(2,4,6-triisopropylbenzoyloxy)ethyl] dithiocarbonate

Guidance literature:: (tributylstannyl)methyl 2,4,6-triisopropylbenzoate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.0833333h; Inert atmosphere;

benzaldehyde; In tetrahydrofuran; hexane; at -78 ℃; for 0.166667h; Inert atmosphere;

carbon disulfide; methyl iodide; Further stages;
DOI:10.1021/jo802625q

Reference yield: 100.0%

: 1133931-92-6
S-methyl O-[1-phenyl-2-(2,4,6-triisopropylbenzoyloxy)ethyl] dithiocarbonate

: 93-56-1
phenylethane 1,2-diol

Guidance literature:: S-methyl O-[1-phenyl-2-(2,4,6-triisopropylbenzoyloxy)ethyl] dithiocarbonate; With lithium aluminium tetrahydride; In tetrahydrofuran; at 70 ℃; for 2h;

With hydrogenchloride; water; In tetrahydrofuran; acetone;
DOI:10.1021/jo802625q