Technology Process of C26H36FN3O2Si
There total 5 articles about C26H36FN3O2Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; ammonium formate;
In
tetrahydrofuran; methanol;
at 20 ℃;
for 2h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tris-(dibenzylideneacetone)dipalladium(0); potassium acetate; tricyclohexylphosphine / 1,4-dioxane / 16 h / 90 °C / Inert atmosphere
2: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / water; 1,2-dimethoxyethane / 16 h / 80 °C / Inert atmosphere
3: lithium chloride; N,N,N,N,N,N-hexamethylphosphoric triamide / 16 h / 110 °C / Inert atmosphere
4: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 17 h / 20 °C / Cooling with ice
5: ammonium formate; palladium 10% on activated carbon / methanol; tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
With
N,N,N,N,N,N-hexamethylphosphoric triamide; tris-(dibenzylideneacetone)dipalladium(0); tetrakis(triphenylphosphine) palladium(0); di-isopropyl azodicarboxylate; palladium 10% on activated carbon; ammonium formate; potassium acetate; potassium carbonate; triphenylphosphine; lithium chloride; tricyclohexylphosphine;
In
tetrahydrofuran; 1,4-dioxane; methanol; 1,2-dimethoxyethane; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / water; 1,2-dimethoxyethane / 16 h / 80 °C / Inert atmosphere
2: lithium chloride; N,N,N,N,N,N-hexamethylphosphoric triamide / 16 h / 110 °C / Inert atmosphere
3: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 17 h / 20 °C / Cooling with ice
4: ammonium formate; palladium 10% on activated carbon / methanol; tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
With
N,N,N,N,N,N-hexamethylphosphoric triamide; tetrakis(triphenylphosphine) palladium(0); di-isopropyl azodicarboxylate; palladium 10% on activated carbon; ammonium formate; potassium carbonate; triphenylphosphine; lithium chloride;
In
tetrahydrofuran; methanol; 1,2-dimethoxyethane; water;