5-(4-methoxycarbonylphenyl)-4,6-dipyrrin

Base Information

Chemical Name:5-(4-methoxycarbonylphenyl)-4,6-dipyrrin
CAS No.:197454-83-4
Molecular Formula:C₁₇H₁₄N₂O₂
Molecular Weight:278.31
Hs Code.:

Synonyms:5-(4-methoxycarbonylphenyl)-4,6-dipyrrin

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Chemical Property of 5-(4-methoxycarbonylphenyl)-4,6-dipyrrin

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Technology Process of 5-(4-methoxycarbonylphenyl)-4,6-dipyrrin

There total 1 articles about 5-(4-methoxycarbonylphenyl)-4,6-dipyrrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 167482-99-7
5-(4-carbomethoxyphenyl)dipyrromethane

: 197454-83-4
5-(4-methoxycarbonylphenyl)-4,6-dipyrrin

Guidance literature:: With 2,3-dicyano-5,6-dichloro-parabenzoquinone; In tetrahydrofuran; chloroform; for 2h; cooling;
DOI:10.1039/b712118k

Reference yield: 93.0%

: [iridium(III)(μ-chloro)(2-phenylpyridine)2]2

: 197454-83-4
5-(4-methoxycarbonylphenyl)-4,6-dipyrrin

: [Ir(CH₃O₂CC₆H₄C(C₄H₃N)(C₄H₃N))(C₁₁H₈N)2]

Guidance literature:: With (C₂H₅)3N; In 2-ethoxy-ethanol; under Ar; NEt3 added to suspn. of iridium complex and dipyrrin deriv. in2-ethoxyethanol, mixt. refluxed for 15 h; evapn. under vac., column chromy. (silica, CH2Cl2);
DOI:10.1021/ic101458r

Reference yield: 87.0%

: 14099-01-5
rhenium(I) pentacarbonyl chloride

: 197454-83-4
5-(4-methoxycarbonylphenyl)-4,6-dipyrrin

: 121-44-8
triethylamine

: 603-35-0
triphenylphosphine

: 1351797-42-6
fac-[Re((C₄H₃N)2CC₆H₄CO₂CH₃)(CO)3(PPh₃)]

Guidance literature:: In toluene; Re complex, C4H3NC(C4H4N)C6H4CO2CH3, and (C2H5)3N heated in toluene, P(C6H5)3 added, heated; evapd. (vac.), chromd.;
DOI:10.1021/ic201877t