tert-butyl [(1S,2S)-2-azido-3-(4-tert-butoxyphenyl)-1-(2-oxoethyl)propoxy]acetate

Base Information

Chemical Name:tert-butyl [(1S,2S)-2-azido-3-(4-tert-butoxyphenyl)-1-(2-oxoethyl)propoxy]acetate
CAS No.:246158-11-2
Molecular Formula:C₂₁H₃₁N₃O₅
Molecular Weight:405.494
Hs Code.:

Synonyms:tert-butyl [(1S,2S)-2-azido-3-(4-tert-butoxyphenyl)-1-(2-oxoethyl)propoxy]acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl [(1S,2S)-2-azido-3-(4-tert-butoxyphenyl)-1-(2-oxoethyl)propoxy]acetate

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Technology Process of tert-butyl [(1S,2S)-2-azido-3-(4-tert-butoxyphenyl)-1-(2-oxoethyl)propoxy]acetate

There total 15 articles about tert-butyl [(1S,2S)-2-azido-3-(4-tert-butoxyphenyl)-1-(2-oxoethyl)propoxy]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 699536-19-1
(4S,5S)-2-azido-6-(4-tert-butoxyphenyl)-4-(4-tert-butoxy-2-oxoethoxy)hexane-1,2-diol

: 246158-11-2
tert-butyl [(1S,2S)-2-azido-3-(4-tert-butoxyphenyl)-1-(2-oxoethyl)propoxy]acetate

Guidance literature:: With lead(IV) acetate; sodium carbonate; In benzene; at 20 ℃; for 3h;
DOI:10.1021/jo0356863

Reference yield: 74.0%

: 246158-10-1
{1-[1-azido-2-(4-tert-butoxy-phenyl)-ethyl]-but-3-enyloxy}-acetic acid tert-butyl ester

: 246158-11-2
tert-butyl [(1S,2S)-2-azido-3-(4-tert-butoxyphenyl)-1-(2-oxoethyl)propoxy]acetate

Guidance literature:: {1-[1-azido-2-(4-tert-butoxy-phenyl)-ethyl]-but-3-enyloxy}-acetic acid tert-butyl ester; With N-methyl-2-indolinone; osmium(VIII) oxide; In tetrahydrofuran; water; acetone; for 2h;

With lead(IV) acetate; sodium carbonate; In benzene; at 0 - 20 ℃; for 3h;
DOI:10.1016/S0040-4039(99)01216-2

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 246158-11-2
tert-butyl [(1S,2S)-2-azido-3-(4-tert-butoxyphenyl)-1-(2-oxoethyl)propoxy]acetate

Guidance literature:: Multi-step reaction with 3 steps

1: NaOH; NBu₄HSO₄ / benzene; H₂O / 1 h

2: 0.88 g / N-methylmorpholine oxide; OsO₄ / H₂O; acetone; tetrahydrofuran / 10 h

3: 85 percent / Na₂CO₃; Pb(OAc)4 / benzene / 3 h / 20 °C

With lead(IV) acetate; sodium hydroxide; osmium(VIII) oxide; tetra(n-butyl)ammonium hydrogensulfate; sodium carbonate; 4-methylmorpholine N-oxide; In tetrahydrofuran; water; acetone; benzene;
DOI:10.1021/jo0356863