3-(2-vinyl-4,5-dimethoxyphenyl)-2-methyl-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline

Base Information

Chemical Name:3-(2-vinyl-4,5-dimethoxyphenyl)-2-methyl-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline
CAS No.:120021-26-3
Molecular Formula:C₂₂H₂₇NO₄
Molecular Weight:369.461
Hs Code.:

Synonyms:3-(2-vinyl-4,5-dimethoxyphenyl)-2-methyl-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(2-vinyl-4,5-dimethoxyphenyl)-2-methyl-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline

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Technology Process of 3-(2-vinyl-4,5-dimethoxyphenyl)-2-methyl-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline

There total 6 articles about 3-(2-vinyl-4,5-dimethoxyphenyl)-2-methyl-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 57129-74-5
(+/-)-N-methylxylopinine iodide

: 120021-26-3
3-(2-vinyl-4,5-dimethoxyphenyl)-2-methyl-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: With potassium hydroxide; In ethanol; for 3h; Heating;
DOI:10.1007/BF00758315

Reference yield:

: 6429-04-5,66820-84-6
1,2,3,4-tetrahydro-1-(3,4-dimethoxybenzyl)-6,7-dimethoxyisoquinoline hydrochloride

: 120021-26-3
3-(2-vinyl-4,5-dimethoxyphenyl)-2-methyl-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / ethanol; H₂O / 8 h / 20 °C

2: 99 percent / ethanol / 24 h / 20 °C

3: 89 percent / KOH / ethanol / 3 h / Heating

With potassium hydroxide; In ethanol; water;
DOI:10.1007/BF00758315

Reference yield:

: 13074-31-2
Tetrahydropapaverine

: 120021-26-3
3-(2-vinyl-4,5-dimethoxyphenyl)-2-methyl-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 4 steps

1: 66 percent / HCl / ethanol

2: 80 percent / ethanol; H₂O / 8 h / 20 °C

3: 99 percent / ethanol / 24 h / 20 °C

4: 89 percent / KOH / ethanol / 3 h / Heating

With hydrogenchloride; potassium hydroxide; In ethanol; water;
DOI:10.1007/BF00758315