2,3,10,11-tetramethoxy-7-methyl-5,8,13,13a-tetrahydro-6H-isoquino[3,2-a]isoquinolinium iodide

Base Information

Chemical Name:2,3,10,11-tetramethoxy-7-methyl-5,8,13,13a-tetrahydro-6H-isoquino[3,2-a]isoquinolinium iodide
CAS No.:57129-74-5
Molecular Formula:C22H28NO4+
Molecular Weight:497.3665
Hs Code.:

Synonyms:2,3,10,11-Tetramethoxy-7-methyl-5,8,13,13a-tetrahydro-6H-isoquino[3,2-a]isoquinolinium;

Suppliers and Price of 2,3,10,11-tetramethoxy-7-methyl-5,8,13,13a-tetrahydro-6H-isoquino[3,2-a]isoquinolinium iodide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 2 raw suppliers

Chemical Property of 2,3,10,11-tetramethoxy-7-methyl-5,8,13,13a-tetrahydro-6H-isoquino[3,2-a]isoquinolinium iodide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,3,10,11-tetramethoxy-7-methyl-5,8,13,13a-tetrahydro-6H-isoquino[3,2-a]isoquinolinium iodide

There total 8 articles about 2,3,10,11-tetramethoxy-7-methyl-5,8,13,13a-tetrahydro-6H-isoquino[3,2-a]isoquinolinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 523-02-4,4216-86-8,6872-27-1,13407-95-9
2,3,10,11-tetramethoxy-5,6,7,8,13,13a-hexahydroisoquinolino[3,2-a]isoquinoline

: 74-88-4
methyl iodide

: 57129-74-5
(+/-)-N-methylxylopinine iodide

Guidance literature:: In ethanol; at 20 ℃; for 24h;
DOI:10.1007/BF00758315

Reference yield:

: 523-02-4,4216-86-8,6872-27-1,13407-95-9
2,3,10,11-tetramethoxy-5,6,7,8,13,13a-hexahydroisoquinolino[3,2-a]isoquinoline

: 74-88-4
methyl iodide

: 52194-51-1,52194-52-2,52194-53-3,52438-48-9,57129-74-5,62860-05-3,62860-06-4,65025-46-9,120052-37-1
(+/-)-Xylopinin-trans-methiodid

: 2,3,10,11-tetramethoxy-7-methyl-5,8,13,13a-tetrahydro-6H-isoquino[3,2-a]isoquinolinium; iodide

Guidance literature:: In chloroform; acetone; at 20 ℃; for 1h;
DOI:10.1016/S0031-9422(03)00497-7

Reference yield:

: 6429-04-5,66820-84-6
1,2,3,4-tetrahydro-1-(3,4-dimethoxybenzyl)-6,7-dimethoxyisoquinoline hydrochloride

: 52194-51-1,52194-52-2,52194-53-3,52438-48-9,57129-74-5,62860-05-3,62860-06-4,65025-46-9,120052-37-1
(+/-)-Xylopinin-trans-methiodid

Guidance literature:: Multi-step reaction with 2 steps

1: 8.2 g / H₂O / 30 h / Heating

2: 122 mg / acetone; CHCl₃ / 1 h / 20 °C

In chloroform; water; acetone;
DOI:10.1016/S0031-9422(03)00497-7