5-Bromo-1-(diethoxymethyl)-2,3-dimethoxybenzene

Base Information

Chemical Name:5-Bromo-1-(diethoxymethyl)-2,3-dimethoxybenzene
CAS No.:128069-95-4
Molecular Formula:C₁₃H₁₉BrO₄
Molecular Weight:319.195
Hs Code.:
DSSTox Substance ID:DTXSID101241674

Synonyms:5-Bromo-1-(diethoxymethyl)-2,3-dimethoxybenzene;DTXSID101241674;128069-95-4

Suppliers and Price of 5-Bromo-1-(diethoxymethyl)-2,3-dimethoxybenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Bromo-1-(diethoxymethyl)-2,3-dimethoxybenzene

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:318.04667
Heavy Atom Count:18
Complexity:221

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOC(C1=C(C(=CC(=C1)Br)OC)OC)OCC

Technology Process of 5-Bromo-1-(diethoxymethyl)-2,3-dimethoxybenzene

There total 3 articles about 5-Bromo-1-(diethoxymethyl)-2,3-dimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 71295-21-1
5-bromo-2,3-dimethoxybenzaldehyde

: 122-51-0
orthoformic acid triethyl ester

: 128069-95-4
5-bromo-2,3-dimethoxybenzaldehyde diethyl acetal

Guidance literature:: With hydrogenchloride; In ethanol; for 0.5h; Heating;

Reference yield:

: 5034-74-2
5-bromo-3-methoxysalicylaldehyde

: 128069-95-4
5-bromo-2,3-dimethoxybenzaldehyde diethyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 1) sodium hydroxide / DMF, 1) 70 deg C, 30 min, 2) 12 h

2: 93 percent / 32 percent HCl / ethanol / 0.5 h / Heating

With hydrogenchloride; sodium hydroxide; In ethanol;

Reference yield:

: 148-53-8
3-methoxy-2-hydroxybenzaldehyde

: 128069-95-4
5-bromo-2,3-dimethoxybenzaldehyde diethyl acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / KBr, bromine / acetic acid; acetic acid / 1) 15 min, 110 deg C, 2) 24 h, r.t.

2: 1) sodium hydroxide / DMF, 1) 70 deg C, 30 min, 2) 12 h

3: 93 percent / 32 percent HCl / ethanol / 0.5 h / Heating

With hydrogenchloride; sodium hydroxide; bromine; potassium bromide; In ethanol; acetic acid;