Technology Process of C11H17NO2
There total 5 articles about C11H17NO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C13H19NO3;
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 1h;
With
water; sodium sulfate;
In
tetrahydrofuran;
at 0 ℃;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / acetonitrile / 18 h / Reflux
2.1: hydroxylamine hydrochloride; sodium acetate / ethanol / 18 h / Reflux
3.1: hydrogen; ammonia / Raney nickel / ethanol; methanol / 20 h / 4395.87 Torr
4.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C
4.2: 0 °C
With
lithium aluminium tetrahydride; hydroxylamine hydrochloride; ammonia; hydrogen; sodium acetate; potassium carbonate;
Raney nickel;
In
tetrahydrofuran; methanol; ethanol; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: aluminum (III) chloride / dichloromethane / 0.75 h / 0 °C
1.2: 15.5 h / 0 - 20 °C
1.3: Cooling
2.1: potassium carbonate / acetonitrile / 18 h / Reflux
3.1: hydroxylamine hydrochloride; sodium acetate / ethanol / 18 h / Reflux
4.1: hydrogen; ammonia / Raney nickel / ethanol; methanol / 20 h / 4395.87 Torr
5.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C
5.2: 0 °C
With
aluminum (III) chloride; lithium aluminium tetrahydride; hydroxylamine hydrochloride; ammonia; hydrogen; sodium acetate; potassium carbonate;
Raney nickel;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; acetonitrile;
