4-Nitro-benzenesulfonic acid (3aR,4R,6aR)-2,2-dimethyl-6-oxo-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

Base Information

Chemical Name:4-Nitro-benzenesulfonic acid (3aR,4R,6aR)-2,2-dimethyl-6-oxo-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester
CAS No.:89747-55-7
Molecular Formula:C₁₄H₁₅NO₉S
Molecular Weight:373.34
Hs Code.:

Synonyms:4-Nitro-benzenesulfonic acid (3aR,4R,6aR)-2,2-dimethyl-6-oxo-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Nitro-benzenesulfonic acid (3aR,4R,6aR)-2,2-dimethyl-6-oxo-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

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Technology Process of 4-Nitro-benzenesulfonic acid (3aR,4R,6aR)-2,2-dimethyl-6-oxo-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

There total 1 articles about 4-Nitro-benzenesulfonic acid (3aR,4R,6aR)-2,2-dimethyl-6-oxo-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 30725-00-9
2,3-O-isopropylidene-D-ribonic-γ-lactone

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 89747-55-7
4-Nitro-benzenesulfonic acid (3aR,4R,6aR)-2,2-dimethyl-6-oxo-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

Guidance literature:: With pyridine; at -23 ℃; for 2.33333h;
DOI:10.1021/jm00372a003

Reference yield: 96.0%

: 89747-55-7
4-Nitro-benzenesulfonic acid (3aR,4R,6aR)-2,2-dimethyl-6-oxo-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

: 4-Nitro-benzenesulfonic acid (2R,3S,4R)-3,4-dihydroxy-5-oxo-tetrahydro-furan-2-ylmethyl ester

Guidance literature:: With trifluoroacetic acid; In water; for 0.633333h;
DOI:10.1021/jm00372a003

Reference yield:

: 89747-55-7
4-Nitro-benzenesulfonic acid (3aR,4R,6aR)-2,2-dimethyl-6-oxo-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

: 89747-25-1
5-O-<(p-aminophenyl)sulfonyl>-D-ribono-1,4-lactone

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / CF₃COOH / H₂O / 0.63 h

2: 0.161 g / H₂ / 10percent Pd/C / dimethylformamide / 2 h / 1603.2 - 1913.4 Torr

With hydrogen; trifluoroacetic acid; palladium on activated charcoal; In water; N,N-dimethyl-formamide;
DOI:10.1021/jm00372a003