2-{[3-cyano-4-(4-methoxyphenyl)-5,6,7,8-tetrahydro-2-quinolinyl]sulfanyl}-N-phenylacetamide

Base Information

Chemical Name:2-{[3-cyano-4-(4-methoxyphenyl)-5,6,7,8-tetrahydro-2-quinolinyl]sulfanyl}-N-phenylacetamide
CAS No.:720676-74-4
Molecular Formula:C₂₅H₂₃N₃O₂S
Molecular Weight:429.543
Hs Code.:
Mol file:720676-74-4.mol

Synonyms:2-[3-cyano-4-(4-methoxy-phenyl)-5,6,7,8-tetrahydro-quinolin-2-ylsulfanyl]-N-phenyl-acetamide

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Chemical Property of 2-{[3-cyano-4-(4-methoxyphenyl)-5,6,7,8-tetrahydro-2-quinolinyl]sulfanyl}-N-phenylacetamide

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Technology Process of 2-{[3-cyano-4-(4-methoxyphenyl)-5,6,7,8-tetrahydro-2-quinolinyl]sulfanyl}-N-phenylacetamide

There total 1 articles about 2-{[3-cyano-4-(4-methoxyphenyl)-5,6,7,8-tetrahydro-2-quinolinyl]sulfanyl}-N-phenylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 117601-23-7
4-(4-methoxyphenyl)-2-sulfanylidene-1,2,5,6,7,8-hexahydroquinoline-3-carbonitrile

: 587-65-5
N-chloroacetyl-aniline

: 720676-74-4
2-[3-cyano-4-(4-methoxy-phenyl)-5,6,7,8-tetrahydro-quinolin-2-ylsulfanyl]-N-phenyl-acetamide

Guidance literature:: With sodium acetate; In ethanol; for 2h; Heating;
DOI:10.1002/jccs.200500136

Reference yield: 93.0%

: 720676-74-4
2-[3-cyano-4-(4-methoxy-phenyl)-5,6,7,8-tetrahydro-quinolin-2-ylsulfanyl]-N-phenyl-acetamide

: 720676-68-6
3-amino-4-(4-methoxy-phenyl)-5,6,7,8-tetrahydro-thieno[2,3-b]quinoline-2-carboxylic acid phenylamide

Guidance literature:: With sodium ethanolate; In ethanol; for 0.0833333h; Heating;
DOI:10.1002/jccs.200500136

Reference yield:

: 720676-74-4
2-[3-cyano-4-(4-methoxy-phenyl)-5,6,7,8-tetrahydro-quinolin-2-ylsulfanyl]-N-phenyl-acetamide

: 5-(4-methoxy-phenyl)-2-phenyl-6,7,8,9-tetrahydro-2H-11-thia-2,3,4,10-tetraaza-benzo[b]fluoren-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / sodium ethanolate / ethanol / 0.08 h / Heating

2: 92 percent / sodium nitrite; acetic acid; H₂SO₄ / H₂O / 0.08 h / 0 °C

With sulfuric acid; sodium ethanolate; acetic acid; sodium nitrite; In ethanol; water; 1: Thorpe-Ziegler cyclisation;
DOI:10.1002/jccs.200500136