2(S)-[(1(S)-phenylethyl)amino]-3-[2,3,4-tribenzyl-α-L-fucopyranosyl]propanoic acid methyl ester

Base Information

• Chemical Name: 2(S)-[(1(S)-phenylethyl)amino]-3-[2,3,4-tribenzyl-α-L-fucopyranosyl]propanoic acid methyl ester
• CAS No.: 288629-21-0
• Molecular Formula: C₃₉H₄₅NO₆
• Molecular Weight: 623.789

Synonyms:2(S)-[(1(S)-phenylethyl)amino]-3-[2,3,4-tribenzyl-α-L-fucopyranosyl]propanoic acid methyl ester

Chemical Property of 2(S)-[(1(S)-phenylethyl)amino]-3-[2,3,4-tribenzyl-α-L-fucopyranosyl]propanoic acid methyl ester

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Technology Process of 2(S)-[(1(S)-phenylethyl)amino]-3-[2,3,4-tribenzyl-α-L-fucopyranosyl]propanoic acid methyl ester

There total 2 articles about 2(S)-[(1(S)-phenylethyl)amino]-3-[2,3,4-tribenzyl-α-L-fucopyranosyl]propanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

methanol (67-56-1) + 2(S)-[(1(S)-phenylethyl)amino]-3-[2,3,4-tribenzyl-α-L-fucopyranosyl]propanenitrile (288629-16-3) → 2(S)-[(1(S)-phenylethyl)amino]-3-[2,3,4-tribenzyl-α-L-fucopyranosyl]propanoic acid methyl ester (288629-21-0)

Guidance literature:

With hydrogenchloride; at 0 ℃; for 2h;

DOI:10.1021/jo000034p

Reference yield:

methanol (67-56-1) + 2-[(1(S)-phenylethyl)amino]-3-[2,3,4-tribenzyl-α-L-fucopyranosyl]propanenitrile → 2(R)-[(1(S)-phenylethyl)amino]-3-[2,3,4-tribenzyl-α-L-fucopyranosyl]propanoic acid methyl ester + 2(S)-[(1(S)-phenylethyl)amino]-3-[2,3,4-tribenzyl-α-L-fucopyranosyl]propanoic acid methyl ester (288629-21-0)

Guidance literature:

With hydrogenchloride; at 0 ℃; for 2h;

DOI:10.1021/jo000034p

Reference yield: 95.0%

2(S)-[(1(S)-phenylethyl)amino]-3-[2,3,4-tribenzyl-α-L-fucopyranosyl]propanoic acid methyl ester (288629-21-0) → 2(S)-[(1(S)-phenylethyl)amino]-3-[2,3,4-tribenzyl-α-L-fucopyranosyl]propanoic acid (288629-19-6)

Guidance literature:

With lithium hydroxide; In methanol; water; at 20 ℃; for 16h; pH=9.5 - 10.5;

DOI:10.1021/jo000034p

upstream raw materials:

methanol

2(S)-[(1(S)-phenylethyl)amino]-3-[2,3,4-tribenzyl-α-L-fucopyranosyl]propanenitrile

Downstream raw materials:

2(S)-[(1(S)-phenylethyl)amino]-3-[2,3,4-tribenzyl-α-L-fucopyranosyl]propanoic acid

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