3-(N-Benzoyl-5-indolyl)methyl-5,7-dimethyl-2-ethyl-3H-imidazo[4,5-b]pyridin

Base Information

Chemical Name:3-(N-Benzoyl-5-indolyl)methyl-5,7-dimethyl-2-ethyl-3H-imidazo[4,5-b]pyridin
CAS No.:145303-53-3
Molecular Formula:C₂₆H₂₄N₄O
Molecular Weight:408.503
Hs Code.:

Synonyms:3-(N-Benzoyl-5-indolyl)methyl-5,7-dimethyl-2-ethyl-3H-imidazo[4,5-b]pyridin

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Chemical Property of 3-(N-Benzoyl-5-indolyl)methyl-5,7-dimethyl-2-ethyl-3H-imidazo[4,5-b]pyridin

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Technology Process of 3-(N-Benzoyl-5-indolyl)methyl-5,7-dimethyl-2-ethyl-3H-imidazo[4,5-b]pyridin

There total 5 articles about 3-(N-Benzoyl-5-indolyl)methyl-5,7-dimethyl-2-ethyl-3H-imidazo[4,5-b]pyridin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 133240-06-9
2-ethyl-5,7-dimethyl-1H-imidazo[4,5-b]pyridine

: 145303-52-2
(5-(bromomethyl)-1H-indol-1-yl)(phenyl)methanone

: 145303-53-3
3-(N-Benzoyl-5-indolyl)methyl-5,7-dimethyl-2-ethyl-3H-imidazo[4,5-b]pyridin

Guidance literature:: With NaH; In hexane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 614-96-0
5-methyl-1H-indole

: 145303-53-3
3-(N-Benzoyl-5-indolyl)methyl-5,7-dimethyl-2-ethyl-3H-imidazo[4,5-b]pyridin

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / 4-(dimethylamino)pyridine, Et₃N / CH₂Cl₂ / 16 h / Ambient temperature

2: 80 percent / N-bromosuccinimide, azoisobutyronitrile / CCl₄ / 4 h / Heating

3: NaH / 1.) DMF, 5 min, 2.) DMF, 2.5 h

With dmap; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sodium hydride; triethylamine; In tetrachloromethane; dichloromethane;
DOI:10.1021/jm00078a013

Reference yield:

: 98-88-4
benzoyl chloride

: 145303-53-3
3-(N-Benzoyl-5-indolyl)methyl-5,7-dimethyl-2-ethyl-3H-imidazo[4,5-b]pyridin

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / 4-(dimethylamino)pyridine, Et₃N / CH₂Cl₂ / 16 h / Ambient temperature

2: 80 percent / N-bromosuccinimide, azoisobutyronitrile / CCl₄ / 4 h / Heating

3: NaH / 1.) DMF, 5 min, 2.) DMF, 2.5 h

With dmap; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sodium hydride; triethylamine; In tetrachloromethane; dichloromethane;
DOI:10.1021/jm00078a013