Technology Process of N-(2,4,6-trichlorophenyl)formamide
There total 1 articles about N-(2,4,6-trichlorophenyl)formamide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
Hexamethyldisiloxane; MS-5Angstroem; 4-(trifluoromethyl)benzoic anhydride; silver trifluoromethanesulfonate; titanium tetrachloride;
In
dichloromethane;
for 20h;
Ambient temperature;
- Guidance literature:
-
With
triethylamine; trichlorophosphate;
In
dichloromethane;
for 0.0666667h;
Cooling with ice;
Green chemistry;
DOI:10.1039/d0gc02722g
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: palladium diacetate; Cy-DHTP*HBF4; lithium tert-butoxide / 1-methyl-pyrrolidin-2-one / 0.5 h / 20 °C / Inert atmosphere
1.2: 2 h / 110 °C / Inert atmosphere
2.1: Cy-DHTP*HBF4; tris-(dibenzylideneacetone)dipalladium(0) / tetrahydrofuran / 24.5 h / 0 - 70 °C / Inert atmosphere
With
tris-(dibenzylideneacetone)dipalladium(0); Cy-DHTP*HBF4; palladium diacetate; lithium tert-butoxide;
In
tetrahydrofuran; 1-methyl-pyrrolidin-2-one;
2.1: |Kumada Cross-Coupling;
DOI:10.1039/c7ob01547j
