1-(5-fluoropyridin-2-yl)-N-(2-methoxy-6-pentadecylbenzyl)-1H-pyrazole-4-sulfonamide

Base Information

Chemical Name:1-(5-fluoropyridin-2-yl)-N-(2-methoxy-6-pentadecylbenzyl)-1H-pyrazole-4-sulfonamide
CAS No.:1375801-10-7
Molecular Formula:C₃₁H₄₅FN₄O₃S
Molecular Weight:572.788
Hs Code.:

Synonyms:1-(5-fluoropyridin-2-yl)-N-(2-methoxy-6-pentadecylbenzyl)-1H-pyrazole-4-sulfonamide

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Chemical Property of 1-(5-fluoropyridin-2-yl)-N-(2-methoxy-6-pentadecylbenzyl)-1H-pyrazole-4-sulfonamide

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Technology Process of 1-(5-fluoropyridin-2-yl)-N-(2-methoxy-6-pentadecylbenzyl)-1H-pyrazole-4-sulfonamide

There total 5 articles about 1-(5-fluoropyridin-2-yl)-N-(2-methoxy-6-pentadecylbenzyl)-1H-pyrazole-4-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.9%

: 1259030-30-2
1-(5-fluoropyridin-2-yl)-1H-pyrazole-4-sulfonyl chloride

: 1363400-50-3
2-methoxy-6-pentadecylphenylmethanamine

: 1375801-10-7
1-(5-fluoropyridin-2-yl)-N-(2-methoxy-6-pentadecylbenzyl)-1H-pyrazole-4-sulfonamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.2174/157017812800233660

Reference yield:

: 1375800-98-8
2-(azidomethyl)-1-methoxy-3-pentadecylbenzene

: 1375801-10-7
1-(5-fluoropyridin-2-yl)-N-(2-methoxy-6-pentadecylbenzyl)-1H-pyrazole-4-sulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / ethanol / 2 h / 3102.97 Torr / Inert atmosphere

2: triethylamine / dichloromethane / 2 h / 0 - 20 °C

With palladium 10% on activated carbon; hydrogen; triethylamine; In ethanol; dichloromethane;
DOI:10.2174/157017812800233660

Reference yield:

: 65446-29-9
2-methoxy-6-pentadecyl-benzoic acid methyl ester

: 1375801-10-7
1-(5-fluoropyridin-2-yl)-N-(2-methoxy-6-pentadecylbenzyl)-1H-pyrazole-4-sulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 18.67 h / 0 - 20 °C

2: triethylamine / dichloromethane / 3.25 h / 0 - 20 °C

3: sodium azide / N,N-dimethyl-formamide / 2 h / 100 °C

4: palladium 10% on activated carbon; hydrogen / ethanol / 2 h / 3102.97 Torr / Inert atmosphere

5: triethylamine / dichloromethane / 2 h / 0 - 20 °C

With lithium aluminium tetrahydride; sodium azide; palladium 10% on activated carbon; hydrogen; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.2174/157017812800233660