bis(8-bromo-6-phenyl-4H-ibenzo[f]midazo[1,5-a][1,4]diazepine-3-carboxy)diethylene glycol diester

Base Information

Chemical Name:bis(8-bromo-6-phenyl-4H-ibenzo[f]midazo[1,5-a][1,4]diazepine-3-carboxy)diethylene glycol diester
CAS No.:612527-43-2
Molecular Formula:C₄₀H₃₀Br₂N₆O₅
Molecular Weight:834.523
Hs Code.:

Synonyms:bis(8-bromo-6-phenyl-4H-ibenzo[f]midazo[1,5-a][1,4]diazepine-3-carboxy)diethylene glycol diester

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Chemical Property of bis(8-bromo-6-phenyl-4H-ibenzo[f]midazo[1,5-a][1,4]diazepine-3-carboxy)diethylene glycol diester

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Technology Process of bis(8-bromo-6-phenyl-4H-ibenzo[f]midazo[1,5-a][1,4]diazepine-3-carboxy)diethylene glycol diester

There total 2 articles about bis(8-bromo-6-phenyl-4H-ibenzo[f]midazo[1,5-a][1,4]diazepine-3-carboxy)diethylene glycol diester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.7%

: 612527-33-0
8-bromo-6-phenyl-4H-benzo[f]imidazo[1,5-a][1,4]diazepine-3-carboxylic acid

: 111-46-6
diethylene glycol

: 612527-43-2
bis(8-bromo-6-phenyl-4H-ibenzo[f]midazo[1,5-a][1,4]diazepine-3-carboxy)diethylene glycol diester

Guidance literature:: 8-bromo-6-phenyl-4H-benzo[f]imidazo[1,5-a][1,4]diazepine-3-carboxylic acid; With 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

diethylene glycol; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.bmc.2008.08.072

Reference yield: 93.7%

: 612527-43-2
bis(8-bromo-6-phenyl-4H-ibenzo[f]midazo[1,5-a][1,4]diazepine-3-carboxy)diethylene glycol diester

Guidance literature:

Reference yield: 49.5%

: 612527-43-2
bis(8-bromo-6-phenyl-4H-ibenzo[f]midazo[1,5-a][1,4]diazepine-3-carboxy)diethylene glycol diester

: 1066-54-2
trimethylsilylacetylene

: 612527-45-4
bis(8-trimethylsilylacetylenyl-6-phenyl-4H-ibenzo[f]midazo[1,5-a][1,4]diazepine-3-carboxy)diethylene glycol diester

Guidance literature:: With bis(acetato)bis(triphenylphosphine)palladium⁽⁰⁾; triethylamine; In acetonitrile; Reflux;
DOI:10.1016/j.bmc.2008.08.072