(3aR,4S,6R,6aS)-6-anililino-2,2-dimethyl-tetrahydro-3aH-cyclopenta[d][1,3]dioxol-4-ol

Base Information

Chemical Name:(3aR,4S,6R,6aS)-6-anililino-2,2-dimethyl-tetrahydro-3aH-cyclopenta[d][1,3]dioxol-4-ol
CAS No.:155855-55-3
Molecular Formula:C₁₄H₁₉NO₃
Molecular Weight:249.31
Hs Code.:

Synonyms:(3aR,4S,6R,6aS)-6-anililino-2,2-dimethyl-tetrahydro-3aH-cyclopenta[d][1,3]dioxol-4-ol

Suppliers and Price of (3aR,4S,6R,6aS)-6-anililino-2,2-dimethyl-tetrahydro-3aH-cyclopenta[d][1,3]dioxol-4-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (3aR,4S,6R,6aS)-6-anililino-2,2-dimethyl-tetrahydro-3aH-cyclopenta[d][1,3]dioxol-4-ol

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (3aR,4S,6R,6aS)-6-anililino-2,2-dimethyl-tetrahydro-3aH-cyclopenta[d][1,3]dioxol-4-ol

There total 9 articles about (3aR,4S,6R,6aS)-6-anililino-2,2-dimethyl-tetrahydro-3aH-cyclopenta[d][1,3]dioxol-4-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 155855-52-0
(1R,2S,6S,7S)-4,4-dimethyl-9-phenyl-3,5,8-trioxa-9-aza-tricyclo[5.2.1.0^2,6]decane

: 155855-55-3
(3aR,4S,6R,6aS)-6-anililino-2,2-dimethyl-tetrahydro-3aH-cyclopenta[d][1,3]dioxol-4-ol

Guidance literature:: With acetic acid; zinc; In diethyl ether; for 48h; Ambient temperature;

Reference yield:

: 38838-06-1
methyl 5-deoxy-5-iodo-2,3-isopropylidene-β-D-ribofuranoside

: 155855-55-3
(3aR,4S,6R,6aS)-6-anililino-2,2-dimethyl-tetrahydro-3aH-cyclopenta[d][1,3]dioxol-4-ol

Guidance literature:: Multi-step reaction with 4 steps

1: Zn / aq. ethanol / 1 h / Heating

2: Na₂CO₃ / aq. ethanol / 20 °C

3: 590 mg / chlorobenzene / 135 °C

4: 78 percent / acetic acid; Zn / diethyl ether / 24 h / 20 °C

With sodium carbonate; acetic acid; zinc; In diethyl ether; ethanol; chlorobenzene;
DOI:10.1021/jo050987t

Reference yield:

: 155934-55-7
(4R,5R)-2,2-dimethyl-5-vinyl-[1,3]dioxolane-4-carbaldehyde

: 155855-55-3
(3aR,4S,6R,6aS)-6-anililino-2,2-dimethyl-tetrahydro-3aH-cyclopenta[d][1,3]dioxol-4-ol

Guidance literature:: Multi-step reaction with 3 steps

1: Na₂CO₃ / aq. ethanol / 20 °C

2: 590 mg / chlorobenzene / 135 °C

3: 78 percent / acetic acid; Zn / diethyl ether / 24 h / 20 °C

With sodium carbonate; acetic acid; zinc; In diethyl ether; ethanol; chlorobenzene;
DOI:10.1021/jo050987t