C₂₀H₂₃Cl₂N₂PPd

Base Information

• Chemical Name: C₂₀H₂₃Cl₂N₂PPd
• CAS No.: 1552317-21-1
• Molecular Formula: C₂₀H₂₃Cl₂N₂PPd
• Molecular Weight: 499.716
• Mol file: 1552317-21-1.mol

Synonyms:C₂₀H₂₃Cl₂N₂PPd

Chemical Property of C₂₀H₂₃Cl₂N₂PPd

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of C₂₀H₂₃Cl₂N₂PPd

There total 2 articles about C₂₀H₂₃Cl₂N₂PPd which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

dichloro bis(acetonitrile) palladium(II) (21264-30-2,90243-59-7,14592-56-4) + C20H23N2P (1552317-18-6) → C20H23Cl2N2PPd (1552317-21-1)

Guidance literature:

In chloroform; for 2h; Inert atmosphere; Reflux; Schlenk technique;

DOI:10.1016/j.tet.2014.01.002

Reference yield:

bis(o-tolyl)chlorophosphine (36042-94-1) + N,N-dimethyl-1H-pyrrol-1-amine (78307-76-3) → C20H23Cl2N2PPd (1552317-21-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / -78 - 20 °C / Inert atmosphere; Schlenk technique

1.2: 0 - 20 °C / Inert atmosphere; Schlenk technique

2.1: chloroform / 2 h / Inert atmosphere; Reflux; Schlenk technique

With n-butyllithium; In tetrahydrofuran; hexane; chloroform;

DOI:10.1016/j.tet.2014.01.002

upstream raw materials:

dichloro bis(acetonitrile) palladium(II)

C₂₀H₂₃N₂P

bis(o-tolyl)chlorophosphine

N,N-dimethyl-1H-pyrrol-1-amine