[3]phenanthryl-o-tolyl ketone

Base Information

• Chemical Name: [3]phenanthryl-o-tolyl ketone
• CAS No.: 859197-18-5
• Molecular Formula: C₂₂H₁₆O
• Molecular Weight: 296.368
• Mol file: 859197-18-5.mol

Synonyms:[3]phenanthryl-o-tolyl ketone

Chemical Property of [3]phenanthryl-o-tolyl ketone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of [3]phenanthryl-o-tolyl ketone

There total 2 articles about [3]phenanthryl-o-tolyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ortho-tolylmagnesium bromide (932-31-0) → [3]phenanthryl-o-tolyl ketone (859197-18-5)

Guidance literature:

With diethyl ether; benzene; anschliessend Behandeln mit wss. Essigsaeure und wss. Salzsaeure und Erhitzen des erhaltenen Reaktionsprodukts mit Wasser;

DOI:10.1021/ja01309a055

Reference yield:

phenanthrene (85-01-8) + ortho-toluoyl chloride (933-88-0) → [3]phenanthryl-o-tolyl ketone (859197-18-5)

Guidance literature:

With aluminium trichloride; nitrobenzene;

DOI:10.1021/ja01309a055

Reference yield:

[3]phenanthryl-o-tolyl ketone (859197-18-5) → benzo[a]naphthacene (226-88-0)

Guidance literature:

at 430 - 450 ℃;

DOI:10.1039/jr9310000489

upstream raw materials:

ortho-tolylmagnesium bromide

phenanthrene

ortho-toluoyl chloride

Downstream raw materials:

benzo[a]naphthacene