7-((1-(2,4-dichlorobenzyl)-1H-1,2,3-triazol-4-yl)methoxy)-4H-chromen-4-one

Base Information

Chemical Name:7-((1-(2,4-dichlorobenzyl)-1H-1,2,3-triazol-4-yl)methoxy)-4H-chromen-4-one
CAS No.:1382038-52-9
Molecular Formula:C₁₉H₁₃Cl₂N₃O₃
Molecular Weight:402.237
Hs Code.:

Synonyms:7-((1-(2,4-dichlorobenzyl)-1H-1,2,3-triazol-4-yl)methoxy)-4H-chromen-4-one

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Chemical Property of 7-((1-(2,4-dichlorobenzyl)-1H-1,2,3-triazol-4-yl)methoxy)-4H-chromen-4-one

Chemical Property:

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Technology Process of 7-((1-(2,4-dichlorobenzyl)-1H-1,2,3-triazol-4-yl)methoxy)-4H-chromen-4-one

There total 4 articles about 7-((1-(2,4-dichlorobenzyl)-1H-1,2,3-triazol-4-yl)methoxy)-4H-chromen-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1348630-12-5
C₁₂H₈O₃

: 20443-99-6
2,4-dichlorobenzyl bromide

: 1382038-52-9
7-((1-(2,4-dichlorobenzyl)-1H-1,2,3-triazol-4-yl)methoxy)-4H-chromen-4-one

Guidance literature:: With sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In dimethyl sulfoxide; at 20 ℃; for 10h;
DOI:10.1016/j.ejmech.2012.04.026

Reference yield:

: 89-84-9
2',4'-dihydroxy-4-acetophenone

: 1382038-52-9
7-((1-(2,4-dichlorobenzyl)-1H-1,2,3-triazol-4-yl)methoxy)-4H-chromen-4-one

Guidance literature:: Multi-step reaction with 4 steps

1: perchloric acid / 8 h / -20 - 20 °C

2: water / 1 h / 100 °C

3: potassium carbonate / acetone / 8 h / Reflux; Inert atmosphere

4: copper(ll) sulfate pentahydrate; sodium azide; sodium L-ascorbate / dimethyl sulfoxide / 10 h / 20 °C

With sodium azide; perchloric acid; copper(ll) sulfate pentahydrate; water; potassium carbonate; sodium L-ascorbate; In dimethyl sulfoxide; acetone;
DOI:10.1016/j.ejmech.2012.04.026

Reference yield:

: 4-Ethoxy-7-hydroxy-chromenylium; perchlorate

: 1382038-52-9
7-((1-(2,4-dichlorobenzyl)-1H-1,2,3-triazol-4-yl)methoxy)-4H-chromen-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: water / 1 h / 100 °C

2: potassium carbonate / acetone / 8 h / Reflux; Inert atmosphere

3: copper(ll) sulfate pentahydrate; sodium azide; sodium L-ascorbate / dimethyl sulfoxide / 10 h / 20 °C

With sodium azide; copper(ll) sulfate pentahydrate; water; potassium carbonate; sodium L-ascorbate; In dimethyl sulfoxide; acetone;
DOI:10.1016/j.ejmech.2012.04.026