tris(bis(1,2-dimethylphosphino)ethane)bis(μ3-sulfido)tris(μ2-sulfido)trichromium

Base Information

Chemical Name:tris(bis(1,2-dimethylphosphino)ethane)bis(μ3-sulfido)tris(μ2-sulfido)trichromium
CAS No.:100681-53-6
Molecular Formula:C₁₈H₄₈Cr₃P₆S₅
Molecular Weight:766.74
Hs Code.:

Synonyms:tris(bis(1,2-dimethylphosphino)ethane)bis(μ3-sulfido)tris(μ2-sulfido)trichromium

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tris(bis(1,2-dimethylphosphino)ethane)bis(μ3-sulfido)tris(μ2-sulfido)trichromium

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Technology Process of tris(bis(1,2-dimethylphosphino)ethane)bis(μ3-sulfido)tris(μ2-sulfido)trichromium

There total 1 articles about tris(bis(1,2-dimethylphosphino)ethane)bis(μ3-sulfido)tris(μ2-sulfido)trichromium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: chromium dichloride

: sodium hydrogen sulfide

: 23936-60-9
1,2-bis(dimethylphosphanyl)ethane

: 100681-53-6
tris(bis(1,2-dimethylphosphino)ethane)bis(μ3-sulfido)tris(μ2-sulfido)trichromium

chromium: 7440-47-3
chromium

Guidance literature:: In methanol; to a soln. of CrCl2 and NaSH in methanol at -78°C excess of phosphine was added, warming slowly to room temp. over ca. 12 h; evapd. to dryness, recrystd. from toluene at -20°C; elem. anal.;
DOI:10.1021/ja00267a057