Technology Process of tris(bis(1,2-dimethylphosphino)ethane)bis(μ3-sulfido)tris(μ2-sulfido)trichromium
There total 1 articles about tris(bis(1,2-dimethylphosphino)ethane)bis(μ3-sulfido)tris(μ2-sulfido)trichromium which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
methanol;
to a soln. of CrCl2 and NaSH in methanol at -78°C excess of phosphine was added, warming slowly to room temp. over ca. 12 h; evapd. to dryness, recrystd. from toluene at -20°C; elem. anal.;
DOI:10.1021/ja00267a057